A kind of UV resin composition, pdlc dimming film and preparation method thereof
A technology of resin composition and dimming film, applied in optics, nonlinear optics, instruments, etc., can solve the problem of high driving voltage of PDLC, achieve the effect of reducing driving voltage and ensuring safety
- Summary
- Abstract
- Description
- Claims
- Application Information
AI Technical Summary
Problems solved by technology
Method used
Image
Examples
Embodiment 1
[0041] This embodiment provides a UV resin composition and a preparation method thereof.
[0042] The UV resin composition of this example is prepared by stirring and mixing the components shown in Table 1 at normal temperature and pressure:
[0043] Table 1
[0044]
[0045]
[0046] The preparation method of the polyurethane acrylate prepolymer used in the present embodiment is as follows:
[0047] Mix and stir 0.5 mole of isophorone diisocyanate, 1.5 mole of hexamethylene diisocyanate, 1 mole of polyether diol and 0.001 mole of dibutyltin dilaurate, raise the temperature to 60°C for 5 hours, monitor the -NCO content, when- When the NCO content is 50%, add 2 moles of hydroxyethyl acrylate and 0.01 moles of 2,6-di-tert-butyl p-cresol to the reaction system in mole fractions sequentially, and continue the reaction until the -NCO content is less than 0.5%, and the condition of 50 ° C is obtained. Urethane acrylate prepolymer with a lower viscosity of 4500-5000cP.
Embodiment 2
[0049] This embodiment provides a UV resin composition and a preparation method thereof.
[0050] The UV resin composition of this embodiment is prepared by stirring and mixing the components shown in Table 2 at normal temperature and pressure:
[0051] Table 2
[0052]
[0053] The preparation method of the polyurethane acrylate prepolymer used in the present embodiment is as follows:
[0054] Mix and stir 1 mole of isophorone diisocyanate, 1 mole of hexamethylene diisocyanate, 1 mole of polyether diol and 0.001 mole of dibutyltin dilaurate, raise the temperature to 60°C for 5 hours, monitor the -NCO content, when- When the NCO content is 50%, add 0.5 mole of hydroxyethyl acrylate, 1.5 mole of hydroxypropyl acrylate and 0.01 mole of 2,6-di-tert-butyl p-cresol to the reaction system in mole fractions successively, and continue the reaction until the -NCO content is less than 0.5% to obtain a polyurethane acrylate prepolymer with a viscosity of 4500-5000 cP at 50°C.
Embodiment 3
[0056] This embodiment provides a UV resin composition and a preparation method thereof.
[0057] The UV resin composition of this example is prepared by stirring and mixing the components in parts by weight shown in Table 3 at normal temperature and pressure:
[0058] table 3
[0059]
[0060] The preparation method of the polyurethane acrylate prepolymer used in the present embodiment is as follows:
[0061] Mix and stir 1 mole of isophorone diisocyanate, 1 mole of hexamethylene diisocyanate, 1 mole of polyether diol and 0.001 mole of dibutyltin dilaurate, raise the temperature to 60°C for 5 hours, monitor the -NCO content, when- When the NCO content is 50%, add 2 moles of hydroxyethyl acrylate and 0.01 moles of 2,6-di-tert-butyl p-cresol to the reaction system in mole fractions sequentially, and continue the reaction until the -NCO content is less than 0.5%, and the condition of 50 ° C is obtained. Urethane acrylate prepolymer with a lower viscosity of 4500-5000cP.
PUM
| Property | Measurement | Unit |
|---|---|---|
| particle diameter | aaaaa | aaaaa |
| haze | aaaaa | aaaaa |
| haze | aaaaa | aaaaa |
Abstract
Description
Claims
Application Information
Login to View More