A kind of preparation method of cement mortar additive for new block wall
A technology for cement mortar and additives, applied in the field of cement mortar additives, can solve the problems of reducing the strength of the mortar, increasing the production cost, increasing the amount of cement, etc., and achieves the effects of increasing the content of soluble silicon, improving the degree of dispersion, and promoting modification.
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Embodiment 1
[0032] A preparation method for a cement mortar additive for a novel block wall, the preparation method comprising the following steps:
[0033] S1, preparation of modified chitosan solution:
[0034]Weigh 1 kg of malic acid, 1 kg of N-hydroxysuccinimine, and 2 kg of chitosan, and add 1% acetic acid dropwise to chitosan under a magnetic stirring condition of 525 r / min until chitosan is completely dissolved, and add to a scale Add 1 mg / mL of 3-ethylcarbodiimide solution to the N-hydroxysuccinimide taken, and magnetically stir at a speed of 500r / min until the N-hydroxysuccinimine is completely dissolved, then weigh the malic acid and Mix chitosan solution and N-hydroxysuccinimine solution, continue to stir evenly with a rotating speed of 525r / min, adjust the pH to 6.25, then add 0.4kg of silane coupling agent, oscillate and disperse for 9min under 190W ultrasonic waves, and get a change Chitosan solution;
[0035] S2, preparation of modified diatomite:
[0036] Weigh 3kg of d...
Embodiment 2
[0040] A preparation method for a cement mortar additive for a novel block wall, the preparation method comprising the following steps:
[0041] S1, preparation of modified chitosan solution:
[0042] Weigh 1 kg of malic acid, 1 kg of N-hydroxysuccinimine, and 2 kg of chitosan, and add 1% acetic acid dropwise to chitosan under a magnetic stirring condition of 500 r / min until chitosan is completely dissolved, and add to a scale Add 1 mg / mL of 3-ethylcarbodiimide solution to the N-hydroxysuccinimide taken, and magnetically stir at a speed of 500r / min until the N-hydroxysuccinimine is completely dissolved, then add malic acid and chitosan Solution and N-hydroxysuccinimide solution were mixed, continued to stir evenly with a rotating speed of 500r / min, adjusted the pH to 6.0, then added 0.4kg of silane coupling agent, oscillated and dispersed under 180W ultrasonic waves for 8min, and obtained modified chitosan sugar solution;
[0043] S2, preparation of modified diatomite:
[0...
Embodiment 3
[0048] A preparation method for a cement mortar additive for a novel block wall, the preparation method comprising the following steps:
[0049] S1, preparation of modified chitosan solution:
[0050] Take by weighing 1kg, N-hydroxysuccinimine 1kg, and chitosan 2kg, add 1% acetic acid dropwise to chitosan under the magnetic stirring condition of 550r / min until chitosan is completely dissolved, and add to the weighed N Add 1mg / mL 3-ethylcarbodiimide solution to -hydroxysuccinimide, stir magnetically at a speed of 550r / min until N-hydroxysuccinimide is completely dissolved, then weigh the malic acid and chitosan Solution and N-hydroxysuccinimide solution were mixed, continued to stir evenly with a rotating speed of 550r / min, adjusted the pH to 6.5, then added 0.4kg of silane coupling agent, oscillated and dispersed under 200W ultrasonic waves for 10min, and obtained modified chitosan solution;
[0051] S2, preparation of modified diatomite:
[0052] Weigh 3kg of diatomite, 1k...
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