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Instant chlorine-containing electrolyte and preparation method thereof

An electrolyte, instant technology, applied in the direction of electrolysis components, electrolysis process, etc., can solve the problems of slow dissolution rate, inconvenient industrialized production of high-efficiency sodium hypochlorite preparation, low efficiency of sodium hypochlorite, etc., achieves simple preparation method, reduces production cost, and improves preparation efficiency Effect

Inactive Publication Date: 2020-11-24
广东省盐业集团广州有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] The process of preparing sodium hypochlorite by electrolysis does not require the upper limit of the concentration of the salt solution. Generally, the higher the concentration of the salt solution, the higher the electrolysis efficiency. According to the physical properties of the salt, the higher the concentration, the slower the dissolution rate. Therefore, if the existing The efficiency of sodium hypochlorite prepared by electrolysis of chlorine-containing electrolyte into a higher concentration of salt solution is low, which brings great inconvenience to the efficient preparation and industrial production of sodium hypochlorite. And the proportion of disintegrants can be made into effervescent salt products that can be quickly dissolved and used for electrolytic preparation of sodium hypochlorite, which can greatly improve the efficiency of electrolytic preparation of sodium hypochlorite solution

Method used

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  • Instant chlorine-containing electrolyte and preparation method thereof
  • Instant chlorine-containing electrolyte and preparation method thereof
  • Instant chlorine-containing electrolyte and preparation method thereof

Examples

Experimental program
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Effect test

Embodiment 1

[0025] The raw material of a kind of instant chlorine-containing electrolyte consists of: refined salt 88g, sodium bicarbonate 9g, citric acid 3g; total amount is based on 100g, wherein refined salt sodium chloride (on a wet basis) content is 99.05%, moisture content It is 0.12%, and the specific gravity is 96% in the range of particle size ≤ 0.85mm.

[0026] A preparation method for an instant chlorine-containing electrolyte, comprising the following steps:

[0027] (1) Take an appropriate amount of refined salt and sieve it, wherein the aperture of the sieve is 0.85 mm to remove large-sized salt particles;

[0028] (2) Sodium bicarbonate is placed in a mortar, ground into powder, and sieved, wherein the aperture of the sieve is 0.85mm, and then the product is placed in a drying dish; citric acid is placed in a mortar, ground into powder, and placed Dry in an electric blast constant temperature drying oven at 78°C for 1 hour, place in a drying dish to cool, and sieve after c...

Embodiment 2

[0035] An instant chlorine-containing electrolyte and a preparation method thereof. The instant chlorine-containing electrolyte is prepared from 70 parts of pulverized washing salt, 15 parts of an acid source, and 15 parts of an alkali source. The preparation method of the instant chlorine-containing electrolyte includes the following step:

[0036] (1) Take an appropriate amount of crushed washing salt, and use a sieve with a pore size of 0.85 mm to carry out sieving treatment to remove large-sized salt particles. On a wet basis, its sodium chloride content is 99.50%, and its moisture content is 0.54 %, particle size ≤0.85mm;

[0037] (2) Potassium bicarbonate is placed in a mortar, ground into powder, and sieved, wherein the aperture of the sieve is 0.85mm, and then the product is placed in a drying dish for drying; tartaric acid is placed in a mortar, ground into powder, and placed in an electric blast constant temperature drying oven at 70 ° C for 1.5 hours, placed in a d...

Embodiment 3

[0042] An instant chlorine-containing electrolyte and a preparation method thereof. The instant chlorine-containing electrolyte is prepared from 80 parts of edible salt, 10 parts of an acid source, and 10 parts of an alkali source. The preparation method of the instant chlorine-containing electrolyte includes the following steps :

[0043] (1) Take an appropriate amount of refined salt, and use a sieve with an aperture of 0.85 mm to carry out sieving treatment to remove large-sized salt grains. The refined salt has a sodium chloride content of 98.9% on a wet basis and a moisture content of 98.9%. The content is 0.98%, the particle size is ≤0.85mm;

[0044] (2) Potassium bicarbonate and potassium carbonate are placed in a mortar, ground into powder, and sieved, wherein the sieve used for sieving has an aperture of 0.85 mm, and then the product is placed in a drying dish; then malic acid is placed in a grinder ground into powder in a bowl, and placed in an electric blast consta...

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Abstract

The invention discloses an instant chlorine-containing electrolyte and a preparation method thereof. The instant chlorine-containing electrolyte is prepared from the components in parts by mass: 60-90parts of edible salt, 1-20 parts of an acid source and 1-20 parts of an alkali source. The preparation method comprises the following steps: (1) the appropriate amount of edible salt is weighed; (2)the acid source and the alkali source are weighed and ground through mortars correspondingly, and then necessary drying, cooling and sieving are conducted; (3) the edible salt and the obtained acid source and alkali source in step (2) are weighed according to the proportion of the instant chlorine-containing electrolyte in step (1) and sequentially added into a stirring device, the stirring deviceis started to mix materials, stirring is stopped after uniform mix, and the materials are dried; and (4) the appropriate quantity of the material obtained in step (3) are taken, molded by a machine,and packaged. The chlorine-containing electrolyte prepared through the method is quickly dissolved, and the preparation efficiency can be greatly improved when the chlorine-containing electrolyte is used for preparing a sodium hypochlorite solution through industrial electrolysis.

Description

technical field [0001] The invention relates to a chlorine-containing electrolyte and a preparation method thereof, in particular to an instant chlorine-containing electrolyte and a preparation method thereof. Background technique [0002] Sodium hypochlorite is a widely used chlorine-containing disinfectant. The current method of preparing sodium hypochlorite is mainly electrolysis. Because sodium hypochlorite solution is not easy to store for a long time, and the transportation is cumbersome and inconvenient. At this stage, sodium hypochlorite generators are often used to prepare sodium hypochlorite by on-site electrolysis, which is about to eat salt. Add the salt salt device to dissolve it into a certain concentration of brine, and then use the electrolytic reaction of the electrode to electrolyze the salt solution into a certain concentration of sodium hypochlorite solution. It is composed of several parts such as device and liquid storage tank. [0003] The process of ...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C25B1/26
CPCC25B1/26
Inventor 周永婧李东旭孙广瑜张阳
Owner 广东省盐业集团广州有限公司