Waterborne polyurethane/acrylate composite emulsion for single-component plastic silver powder paint and preparation method thereof
A water-based polyurethane and acrylate technology, applied in the direction of coating, can solve the problems of poor performance and demulsification, and achieve the effects of improving alcohol resistance, increasing crosslinking density, and improving water resistance
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Embodiment 1
[0031] The preparation method of the water-based polyurethane / acrylic ester composite emulsion for the one-component plastic silver powder paint provided in the present embodiment is as follows:
[0032] (1) Put 6% PNA1000 in the reactor and vacuum dehydrate at 120°C for 2h, then drop the temperature to 60°C, add 2% HDI and 0.178% DHPA, then slowly raise the temperature to 80°C until the NCO content reaches the theoretical value (two normal Butylamine method titration), then add 0.36% BDO to carry out chain extension, when the NCO content reaches the theoretical value, cool down to 50 ° C and add 0.081% BO and 0.13% 4-HBA, react until the NCO content is 0. Add 10% of the total amount of mixed monomers (mixed monomers are composed of 24.25% MMA, 3.75% IBOMA, 0.4% BA, 0.45% AA and 1.2% DAAM) to reduce the viscosity, and add 23% pure water to disperse to obtain unilateral ethylene Group-terminated polyurethane prepolymer.
[0033] (2) After adding 30% of the total amount of 0.01...
Embodiment 2
[0036] The preparation method of the water-based polyurethane / acrylic ester composite emulsion for one-component plastic silver powder paint provided in this embodiment is consistent with that in Example 1, the difference is that the raw materials and additions used are different from those in Example 1 , the specific formula is shown in Table 2.
Embodiment 3
[0038]The preparation method of the water-based polyurethane / acrylic ester composite emulsion for one-component plastic silver powder paint provided in this embodiment is consistent with that in Example 1, the difference is that the raw materials and additions used are different from those in Example 1 , the specific formula is shown in Table 2.
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