Preparation method and application of biomass-based carbon nanosheet/epoxy composite coating
A technology of carbon nanosheets and composite coatings, applied in the direction of epoxy resin coatings, coatings, nano-carbons, etc., can solve the problems of a large number of holes, low corrosion resistance level, poor physical isolation performance of coatings, etc., and achieve fast corrosion speed , Excellent anti-corrosion performance, and the effect of improving the protection performance
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specific Embodiment approach 1
[0034] Specific embodiment one: the preparation method of a kind of biomass-based carbon nanosheet / epoxy composite coating in this embodiment is completed according to the following steps:
[0035] 1. Pretreatment of biomass powder:
[0036] ①. First, the wheat straw is cleaned, then dried to constant weight, pulverized with a pulverizer, and then sieved to obtain wheat straw powder with a particle size of 75 μm;
[0037] ② Put wheat straw powder with a particle size of 75 μm, deionized water, hydrogen peroxide solution and acetic acid into the reactor, stir evenly, and then seal the reactor; heat the sealed reactor from room temperature to 80°C to 200°C ℃, and then keep warm at 80℃~200℃ for 2h~24h, and cool to room temperature to obtain the reacted wheat straw powder;
[0038] The mass ratio of deionized water, hydrogen peroxide solution, acetic acid and wheat straw powder with a particle size of 75 μm described in step 1.2 is (20~50):(5~20):(1~10):1;
[0039] ③. First, use...
specific Embodiment approach 2
[0057] Specific embodiment 2: The difference between this embodiment and specific embodiment 1 is: the drying temperature described in step 1 ① is 60°C; in step 1 ①, the wheat straw is first cleaned with distilled water until the distilled water is free of turbidity, and then Dry at 60°C to constant weight, pulverize with a pulverizer, and then sieve with a 200-mesh stainless steel screen to obtain wheat straw powder with a particle size of 75 μm. Other steps are the same as in the first embodiment.
specific Embodiment approach 3
[0058] Specific embodiment three: the difference between this embodiment and specific embodiment one or two is: the mass fraction of the hydrogen peroxide solution described in step 1.2 is 5%~20%; the acetic acid described in step 1.2. The mass fraction of the mixture is 5% to 40%; in step 1, the rate of heating the sealed reactor from room temperature to 80°C to 200°C is 1°C / min to 10°C / min. Other steps are the same as those in Embodiment 1 or 2.
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