Preparation method of peony buccal tablets containing omega-3 linolenic acid
A production method and technology of linolenic acid, which are applied in the functions of food ingredients, food extraction, food science and other directions, can solve the problems that the human body is not easy to supplement, the linseed oil is easily oxidized, and cannot be resistant to high temperature cooking, etc. The effect of convenient storage and consumption
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Embodiment 1
[0019] A preparation method of peony buccal tablets containing omega-3 linolenic acid is as follows:
[0020] Step 1. Dry the peony seeds and linseeds at a temperature of 35 degrees Celsius for 20 minutes, control the moisture content at 10%, and pulverize them into a mixed powder of 20-30 meshes;
[0021] Step 2, preparation of mixed fatty acids: mix oil and caustic soda at 80° C. for saponification for 1 hour, cool rapidly, and acidify the lower layer of the extract, namely the water layer, with 10% HCl to a pH of 2-3, extract with petroleum ether, and wash with water until Neutral, and the filtrate is evaporated under reduced pressure to obtain mixed fatty acids in oil;
[0022] Step 3. Mix the mixed powder obtained in Step 1 with mixed fatty acid and acetone, freeze at a certain low temperature for a certain period of time, perform vacuum filtration to remove saturated fatty acid, and distill acetone at 40°C under vacuum conditions to obtain purified ω- 3 linolenic acid; ...
Embodiment 2
[0026] A preparation method of peony buccal tablets containing omega-3 linolenic acid is as follows:
[0027] Step 1. Dry the peony seeds and linseeds at a temperature of 50 degrees Celsius for 10 minutes, control the moisture content at 6%, and pulverize them into a mixed powder of 20-30 mesh;
[0028] Step 2, preparation of mixed fatty acids: mix oil and caustic soda at 80° C. for saponification for 1 hour, cool rapidly, and acidify the lower layer of the extract, namely the water layer, with 10% HCl to a pH of 2-3, extract with petroleum ether, and wash with water until Neutral, and the filtrate is evaporated under reduced pressure to obtain mixed fatty acids in oil;
[0029] Step 3. Mix the mixed powder obtained in Step 1 with mixed fatty acid and acetone, freeze at a certain low temperature for a certain period of time, perform vacuum filtration to remove saturated fatty acid, and distill acetone at 40°C under vacuum conditions to obtain purified ω- 3 linolenic acid;
...
Embodiment 3
[0033] A preparation method of peony buccal tablets containing omega-3 linolenic acid is as follows:
[0034] Step 1. Dry the peony seeds and linseeds at a temperature of 40 degrees Celsius for 15 minutes, control the moisture content at 8%, and pulverize them into a mixed powder of 20-30 meshes;
[0035] Step 2, preparation of mixed fatty acids: mix oil and caustic soda at 80° C. for saponification for 1 hour, cool rapidly, and acidify the lower layer of the extract, namely the water layer, with 10% HCl to a pH of 2-3, extract with petroleum ether, and wash with water until Neutral, and the filtrate is evaporated under reduced pressure to obtain mixed fatty acids in oil;
[0036] Step 3. Mix the mixed powder obtained in Step 1 with mixed fatty acid and acetone, freeze at a certain low temperature for a certain period of time, perform vacuum filtration to remove saturated fatty acid, and distill acetone at 40°C under vacuum conditions to obtain purified ω- 3 linolenic acid; ...
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