Anti-freezing asphalt pavement material and preparation method thereof
A technology of asphalt pavement and asphalt, which is applied in the field of antifreeze asphalt pavement materials and its preparation, can solve the problems of further improvement in performance stability and antifreeze effect, so as to improve transportation efficiency and traffic safety, improve frost resistance and waterproof The effect, the effect of the simple and easy preparation method
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Embodiment 1
[0028] An antifreeze asphalt pavement material is characterized in that it is made of the following raw materials in parts by weight: 60 parts of asphalt, 10 parts of vinyl-terminated fluorosilicone oil, 2-naphthylamine-3,6,8-trisulfonic acid 3 2 parts of epoxy-modified bis(2-hydroxyethyl)amino(trimethylol)methane, 5 parts of carboxylated butyl rubber, 4 parts of amino-terminated hyperbranched polybenzimidazole, 3 parts of pig hair fiber part, 0.5 part of graphene nanosheet, and 2 parts of phosphorus pentoxide; the length of the pig hair fiber is 3 μm.
[0029] The preparation method of described epoxy-modified bis(2-hydroxyethyl)amino(trimethylol)methane comprises the steps of: mixing epichlorohydrin, bis(2-hydroxyethyl)amino(trimethylol) Base) methane was added in the organic solvent, stirred and reacted at 25°C for 4 hours, and then the solvent was removed by rotary evaporation to obtain epoxy-modified bis(2-hydroxyethyl)amino(trimethylol)methane; the ring The molar ratio ...
Embodiment 2
[0032] An antifreeze asphalt pavement material is characterized in that it is made of the following raw materials in parts by weight: 60-80 parts of asphalt, 12 parts of vinyl-terminated fluorosilicone oil, 2-naphthylamine-3,6,8-trisulfone 3-6 parts of acid, 2.3 parts of epoxy-modified bis(2-hydroxyethyl)amino(trimethylol)methane, 6 parts of carboxylated butyl rubber, 5 parts of amino-terminated hyperbranched polybenzimidazole, 3.5 parts of pig hair fibers, 0.7 parts of graphene nanosheets, and 2.5 parts of phosphorus pentoxide; the length of the pig hair fibers is 5 μm.
[0033] The preparation method of described epoxy-modified bis(2-hydroxyethyl)amino(trimethylol)methane comprises the steps of: mixing epichlorohydrin, bis(2-hydroxyethyl)amino(trimethylol) Base) methane was added in the organic solvent, stirred and reacted at 27°C for 4.5 hours, and then the solvent was removed by rotary evaporation to obtain epoxy-modified bis(2-hydroxyethyl)amino(trimethylol)methane; the r...
Embodiment 3
[0036] An antifreeze asphalt pavement material is characterized in that it is made of the following raw materials in parts by weight: 60-80 parts of asphalt, 15 parts of vinyl-terminated fluorosilicone oil, 2-naphthylamine-3,6,8-trisulfone 4.5 parts of acid, 2.5 parts of epoxy-modified bis(2-hydroxyethyl)amino(trimethylol)methane, 7.5 parts of carboxylated butyl rubber, 6 parts of amino-terminated hyperbranched polybenzimidazole, pig hair 4 parts of fiber, 1 part of graphene nanosheet, and 3 parts of phosphorus pentoxide; the length of the pig hair fiber is 6 μm.
[0037] The preparation method of described epoxy-modified bis(2-hydroxyethyl)amino(trimethylol)methane comprises the steps of: mixing epichlorohydrin, bis(2-hydroxyethyl)amino(trimethylol) Base) methane was added in the organic solvent, stirred and reacted at 30°C for 5 hours, and then the solvent was removed by rotary evaporation to obtain epoxy-modified bis(2-hydroxyethyl)amino(trimethylol)methane; the ring The m...
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