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Simple liquid alkali-free setting accelerator and preparation method thereof

A technology of quick-setting agent and liquid, which is applied in the field of preparation of simple liquid non-alkali quick-setting agent, quick-setting agent, and the liquid non-alkali quick-setting agent. The preparation process is simple and the setting time is sufficient

Inactive Publication Date: 2021-03-30
刘翠芬
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] The above technologies have not given specific guidance on how to make the liquid alkali-free accelerator be produced under relatively simple preparation process conditions, and at the same time ensure that the setting time of the alkali-free accelerator meets the national standard

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0018] Embodiment 1: The simple liquid alkali-free quick-setting agent of the present invention is made from the following components and the raw materials of mass fraction: 160 parts of tap water, 30 parts of mineral powder, 250 parts of aluminum sulfate, 10 parts of organic amine , 5 parts of organic acid, 30 parts of fluorosilicon compound, 7 parts of suspending agent. The mineral powder is a combination of 10 parts of kaolin and 20 parts of calcium aluminate, and the particle size of the mineral powder is 100 mesh; the organic amine is 3 parts of triisopropanolamine, 3 parts of diethylenetriamine, A combination of 4 parts of triethanolamine; the organic acid is oxalic acid; the fluorosilicon compound is a combination of 20 parts of ammonium fluorosilicate and 10 parts of zinc fluorosilicate; the suspension The agent is diatomaceous earth.

[0019] The preparation method of described simple and easy liquid alkali-free quick-setting agent comprises the following process ste...

Embodiment 2

[0020] Embodiment 2: The simple liquid alkali-free quick-setting agent of the present invention is made of the following components and the raw materials of mass fraction: 200 parts of tap water, 40 parts of mineral powder, 275 parts of aluminum sulfate, 20 parts of organic amine , 3 parts of organic acid, 40 parts of fluorosilicon compound, 7 parts of suspending agent. The mineral powder is a combination of 20 parts of kaolin and 20 parts of calcium carbonate, and the particle size of the mineral powder is 500 mesh; the organic amine is a mixture of 10 parts of triisopropanolamine and 10 parts of triethanolamine. combination; the organic acid is malic acid; the fluorosilicon compound is zinc fluorosilicate; the suspending agent is hydrated magnesium silicate superfine powder.

[0021] The preparation method of described simple and easy liquid alkali-free quick-setting agent comprises the following process steps: (1) add 200 parts of water, 40 parts of mineral powder, and 275 ...

Embodiment 3

[0022]Embodiment 3: The simple liquid alkali-free quick-setting agent of the present invention is made from the following components and the raw materials of mass fraction: 175 parts of tap water, 30 parts of mineral powder, 240 parts of aluminum sulfate, 30 parts of organic amine , 4 parts of organic acid, 50 parts of fluorosilicon compound, and 5 parts of suspending agent. The mineral powder is a combination of 10 parts of kaolin and 20 parts of calcium carbonate. The particle size of the mineral powder is 325 mesh; the organic amine is 10 parts of diethylenetriamine, 15 parts of triethylenetetramine, A combination of three raw materials of triethanolamine; the organic acid is tartaric acid; the fluorosilicon compound is a combination of 20 parts of fluorosilicic acid and 30 parts of zinc fluorosilicate; the suspending agent is diatomaceous earth .

[0023] The preparation method of described simple and easy liquid alkali-free quick-setting agent comprises the following pro...

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Abstract

The invention discloses a simple liquid alkali-free setting accelerator and a preparation method thereof. The setting accelerator comprises the following raw material components in parts by mass: 300-400 parts of tap water, 20-60 parts of mineral powder, 450-550 parts of aluminum sulfate, 20-60 parts of organic amine, 1-10 parts of organic acid, 50-100 parts of fluorine-silicon compound and 5-20 parts of a suspending agent. The mineral powder is one or two of kaolin, bauxite, calcium aluminate and calcium carbonate, and the particle size of the mineral powder is 100-500 meshes; the organic amine is one or more of triisopropanolamine, diethylenetriamine, triethylene tetramine and triethanolamine; the fluorine-silicon compound is one or two of fluosilicic acid, ammonium fluosilicate and zincfluosilicate; and the suspending agent is ultrafine powder of diatomite, bentonite and hydrated magnesium silicate. The invention also provides a preparation method of the accelerator. The inventionrelates to a liquid alkali-free setting accelerator containing polyaluminum sulfate, which can be produced under simple preparation process conditions, and simultaneously confirms that the setting time of the alkali-free setting accelerator meets the national standard.

Description

technical field [0001] The invention relates to an accelerator for concrete, in particular to a simple liquid alkali-free accelerator. The invention belongs to the technical field of building material chemical admixtures. The invention also relates to a preparation method of the liquid alkali-free accelerator. Background technique [0002] In recent years, a large number of infrastructure constructions, such as tunnels, railways and other infrastructure projects, have greatly increased the demand for accelerators. In the concrete or mortar system, the alkali-free quick-setting agent forms calcium aluminate hydrate or calcium sulfoaluminate hydrate and other substances through the large amount of aluminum ions contained in the solution and cement, so that the concrete or mortar can be set and hardened in a short time. At present, the liquid alkali-free accelerators on the market are basically products with aluminum sulfate as the main component, but the solubility of alumin...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C04B24/12C04B103/12
CPCC04B40/0039C04B2103/12C04B22/148C04B24/08C04B24/10C04B24/122C04B24/121C04B24/04C04B22/126
Inventor 田遥赵明敏黄玉美刘昭洋贾二鹏王龙飞李茜茜刘翠芬
Owner 刘翠芬