Preparation method of modified magnesium oxide composite polishing powder
A composite polishing and magnesium oxide technology, which is applied in the field of polishing powder, can solve the problems of affecting the cutting force of the product, insufficient sediment reaction, uneven particle dispersion, etc., to achieve the effect of promoting complete reaction, improving polishing performance, and improving performance
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Embodiment 1
[0051] The preparation method of modified magnesium oxide composite polishing powder comprises the following steps:
[0052] Step 1, mix 57kg magnesium chloride, 7.6kg lanthanum chloride, 6.3kg cerium chloride, 5.2kg praseodymium chloride into a solution, then mix with 85kg fluorine-containing potassium hydroxide solution, and in the fluorine-containing potassium hydroxide The volume fraction of potassium is 10%, and the mass concentration ratio of fluoride ion to potassium hydroxide is 1:2 to obtain a precursor solution;
[0053] Step 2, put the precursor solution of step 1 into the ice bath in advance, control the system temperature to be 5 ℃, add 18kg polyethylene glycol solution and 1kg pyridine, then dropwise add 34kg p-toluenesulfonyl chloride, and stir synchronously. , let stand for 1h, and then heat and age for 2d at a temperature of 50 °C, and the precursor is precipitated after filtration;
[0054] Step 3: The precursor is deposited in a high-temperature furnace, ca...
Embodiment 2
[0056] The preparation method of modified magnesium oxide composite polishing powder comprises the following steps:
[0057] Step 1, mix 64kg magnesium chloride, 6.5kg lanthanum chloride, 4.6kg cerium chloride, 6.3kg praseodymium chloride into a solution, then mix with 74kg fluorine-containing potassium hydroxide solution, and in the fluorine-containing potassium hydroxide The volume fraction of potassium is 12%, and the mass concentration ratio of fluoride ion to potassium hydroxide is 2:3 to obtain a precursor solution;
[0058] Step 2, put the precursor solution of step 1 into an ice bath in advance, control the temperature of the system to be 10 ° C, add 13kg polyethylene glycol solution and 3kg pyridine, then dropwise add 28kg p-toluenesulfonyl chloride, and stir synchronously. , let stand for 2h, then heat preservation and aging for 3d at a temperature of 60°C, and the precursor is precipitated after filtration;
[0059] Step 3: The precursor is deposited in a high-temp...
Embodiment 3
[0061]The preparation method of modified magnesium oxide composite polishing powder comprises the following steps:
[0062] Step 1, mix 62kg magnesium chloride, 5.8kg lanthanum chloride, 5.3kg cerium chloride, 7.2kg praseodymium chloride into a solution, then mix with 95kg fluorine-containing potassium hydroxide solution, and in the fluorine-containing potassium hydroxide The volume fraction of potassium is 10%, and the mass concentration ratio of fluoride ion to potassium hydroxide is 1:2 to obtain a precursor solution;
[0063] Step 2, put the precursor solution of step 1 into the ice bath in advance, control the temperature of the system to be 10 ° C, add 15kg polyethylene glycol solution and 2kg pyridine, then dropwise add 30kg p-toluenesulfonyl chloride, and stir synchronously. , let stand for 1h, then heat preservation and aging for 2d at a temperature of 80 °C, and the precursor is precipitated after filtration;
[0064] Step 3: The precursor is deposited in a high-tem...
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