Looking for breakthrough ideas for innovation challenges? Try Patsnap Eureka!

Preparation method of modified magnesium oxide composite polishing powder

A composite polishing and magnesium oxide technology, which is applied in the field of polishing powder, can solve the problems of affecting the cutting force of the product, insufficient sediment reaction, uneven particle dispersion, etc., to achieve the effect of promoting complete reaction, improving polishing performance, and improving performance

Active Publication Date: 2021-10-29
深圳市瑞来稀土材料有限公司
View PDF3 Cites 0 Cited by
  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] During the preparation process of the current magnesium oxide composite polishing powder, the particles in the precursor slurry are not uniformly dispersed, and agglomerated particles are easily produced, and the molecular surface inside the particles is wrapped, resulting in insufficient reaction of the precipitate and affecting the cutting force of the product.

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
View more

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0051] The preparation method of modified magnesium oxide composite polishing powder comprises the following steps:

[0052] Step 1, mix 57kg magnesium chloride, 7.6kg lanthanum chloride, 6.3kg cerium chloride, 5.2kg praseodymium chloride into a solution, then mix with 85kg fluorine-containing potassium hydroxide solution, and in the fluorine-containing potassium hydroxide The volume fraction of potassium is 10%, and the mass concentration ratio of fluoride ion to potassium hydroxide is 1:2 to obtain a precursor solution;

[0053] Step 2, put the precursor solution of step 1 into the ice bath in advance, control the system temperature to be 5 ℃, add 18kg polyethylene glycol solution and 1kg pyridine, then dropwise add 34kg p-toluenesulfonyl chloride, and stir synchronously. , let stand for 1h, and then heat and age for 2d at a temperature of 50 °C, and the precursor is precipitated after filtration;

[0054] Step 3: The precursor is deposited in a high-temperature furnace, ca...

Embodiment 2

[0056] The preparation method of modified magnesium oxide composite polishing powder comprises the following steps:

[0057] Step 1, mix 64kg magnesium chloride, 6.5kg lanthanum chloride, 4.6kg cerium chloride, 6.3kg praseodymium chloride into a solution, then mix with 74kg fluorine-containing potassium hydroxide solution, and in the fluorine-containing potassium hydroxide The volume fraction of potassium is 12%, and the mass concentration ratio of fluoride ion to potassium hydroxide is 2:3 to obtain a precursor solution;

[0058] Step 2, put the precursor solution of step 1 into an ice bath in advance, control the temperature of the system to be 10 ° C, add 13kg polyethylene glycol solution and 3kg pyridine, then dropwise add 28kg p-toluenesulfonyl chloride, and stir synchronously. , let stand for 2h, then heat preservation and aging for 3d at a temperature of 60°C, and the precursor is precipitated after filtration;

[0059] Step 3: The precursor is deposited in a high-temp...

Embodiment 3

[0061]The preparation method of modified magnesium oxide composite polishing powder comprises the following steps:

[0062] Step 1, mix 62kg magnesium chloride, 5.8kg lanthanum chloride, 5.3kg cerium chloride, 7.2kg praseodymium chloride into a solution, then mix with 95kg fluorine-containing potassium hydroxide solution, and in the fluorine-containing potassium hydroxide The volume fraction of potassium is 10%, and the mass concentration ratio of fluoride ion to potassium hydroxide is 1:2 to obtain a precursor solution;

[0063] Step 2, put the precursor solution of step 1 into the ice bath in advance, control the temperature of the system to be 10 ° C, add 15kg polyethylene glycol solution and 2kg pyridine, then dropwise add 30kg p-toluenesulfonyl chloride, and stir synchronously. , let stand for 1h, then heat preservation and aging for 2d at a temperature of 80 °C, and the precursor is precipitated after filtration;

[0064] Step 3: The precursor is deposited in a high-tem...

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

PUM

PropertyMeasurementUnit
particle sizeaaaaaaaaaa
Login to View More

Abstract

This application relates to the technical field of polishing powder, and specifically discloses a preparation method of modified magnesium oxide composite polishing powder. The preparation method is as follows: step 1, mixing magnesium chloride, lanthanum chloride, cerium chloride, and praseodymium chloride into a solution, and then Mix with a fluorine-containing strong alkali solution to obtain a precursor solution; step 2, add pyridine, polyethylene glycol and p-toluenesulfonyl chloride to the above precursor solution, and then keep it warm at a temperature of 50°C-80°C After 2d-3d, the precursor precipitate is obtained after filtration; step 3, the precursor precipitate is placed in a high-temperature furnace, burned at a temperature of 900-1100°C, and then dispersed and classified to obtain modified oxidation Magnesium composite polishing powder. In this application, potassium p-benzenesulfonate and polyethylene glycol are used to generate ester groups with leaving and dispersing functions to improve the uniform dispersion of components in the precursor solution, thereby improving the cutting strength, yield and service life of the polishing powder as a whole .

Description

technical field [0001] The present application relates to the field of polishing powder, more particularly, it relates to a preparation method of modified magnesium oxide composite polishing powder. Background technique [0002] Because of its unique physical and chemical properties, rare earth polishing powder is widely used in lenses, flat glass, glass bulbs, glasses, watch cases and other fields, and also in functional ceramics, catalysts, luminescence, gas sensors, fuel cells and ultraviolet absorption has also been widely used. Due to the limited rare earth resources, in order to reduce the proportion of polishing powder in the rare earth resources, the resource-rich magnesium oxide is generally used as the main component. [0003] In the preparation process of the current magnesium oxide composite polishing powder, the particles in the precursor slurry are not uniformly dispersed, and agglomerated particles are easily generated, and the molecular surface inside the pa...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

Application Information

Patent Timeline
no application Login to View More
Patent Type & Authority Patents(China)
IPC IPC(8): C09G1/02
CPCC09G1/02
Inventor 张俊生
Owner 深圳市瑞来稀土材料有限公司
Who we serve
  • R&D Engineer
  • R&D Manager
  • IP Professional
Why Patsnap Eureka
  • Industry Leading Data Capabilities
  • Powerful AI technology
  • Patent DNA Extraction
Social media
Patsnap Eureka Blog
Learn More
PatSnap group products