Looking for breakthrough ideas for innovation challenges? Try Patsnap Eureka!

Flame-retardant polyamide fabric and preparation method thereof

A fabric and nylon technology is applied in the field of flame retardant nylon fabric and its preparation, which can solve the problems of nylon degradation and deep color, and achieve the effects of less environmental pollution, simple production process and low price.

Pending Publication Date: 2021-04-30
WUHAN TEXTILE UNIV
View PDF8 Cites 0 Cited by
  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Because the active amide bonds in nylon are easy to chemically react with flame retardants, and the hydrogen halides produced by additives at high temperatures will cause problems such as degradation of nylon and deep color

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
View more

Image

Smart Image Click on the blue labels to locate them in the text.
Viewing Examples
Smart Image
  • Flame-retardant polyamide fabric and preparation method thereof
  • Flame-retardant polyamide fabric and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0024] A kind of preparation method of flame-retardant nylon fabric of the present embodiment, described preparation method comprises the following steps:

[0025] (1) Reaction of chloropropyl-POSS with acrylamide: Dissolve 6g of chloropropyl-POSS and 1.5g of triethylamine in 150mL of tetrahydrofuran in a four-neck flask, stir in an ice bath and pass through N 2 For protection, dissolve 5g of acrylamide in 100mL of tetrahydrofuran, add the tetrahydrofuran dissolved in acrylamide dropwise into the tetrahydrofuran dissolved in chloropropyl, the rate of addition is 1 drop / second, after the addition is completed, react in an ice bath at constant temperature, and the reaction time is: After 7 hours, after the reaction was completed, suction filtration under reduced pressure, rotary evaporation, and drying gave the POSS compound containing double bonds.

[0026] (2) Polymerization reaction: Weigh 2 grams of the double bond-containing POSS compound prepared in step (1), dissolve it i...

Embodiment 2

[0029] A kind of preparation method of flame-retardant nylon fabric of the present embodiment, described preparation method comprises the following steps:

[0030] (1) Reaction of chloropropyl-POSS with acrylamide: Dissolve 5g of chloropropyl-POSS and 1g of triethylamine in 150mL of tetrahydrofuran in a four-neck flask, stir in an ice bath and pass through N 2 For protection, dissolve 4g of acrylamide in 100mL of tetrahydrofuran, add the tetrahydrofuran with acrylamide solution into the tetrahydrofuran with chloropropyl group dropwise, the rate of addition is 1 drop / second, after the addition is completed, react in an ice bath at constant temperature, and the reaction time is: After 5 hours, after the reaction was completed, vacuum filtration, rotary evaporation, and drying were performed to obtain a POSS compound containing a double bond.

[0031] (2) Polymerization reaction: Weigh 1 gram of the double bond-containing POSS compound prepared in step (1), dissolve it in 50 mL o...

Embodiment 3

[0034] A kind of preparation method of flame-retardant nylon fabric of the present embodiment, described preparation method comprises the following steps:

[0035] (1) Reaction of chloropropyl-POSS with acrylamide: Dissolve 7g of chloropropyl-POSS and 2g of triethylamine in 150mL of tetrahydrofuran in a four-neck flask, stir in an ice bath and pass through N 2For protection, dissolve 6g of acrylamide in 100mL of tetrahydrofuran, add the tetrahydrofuran dissolved in acrylamide dropwise into the tetrahydrofuran dissolved in chloropropyl group, and the dropping rate is 1 drop / second. After 9 hours, after the reaction was completed, suction filtration under reduced pressure, rotary evaporation, and drying gave the POSS compound containing double bonds.

[0036] (2) Polymerization reaction: Weigh 3 grams of the double bond-containing POSS compound prepared in step (1), dissolve it in 50 mL of dimethylformamide; add 200 mL of distilled water to a four-neck flask, add 12 g of 2-acryl...

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

PUM

No PUM Login to View More

Abstract

The invention relates to a flame-retardant polyamide fabric and a preparation method thereof. The fabric is characterized by being prepared by the following steps of firstly, reacting chloropropyl-POSS with acrylamide to prepare a POSS compound containing double bonds; carrying out a polymerization reaction on the POSS compound containing the double bonds, 2-acrylamide-2-methyl propanesulfonic acid, acrylic acid and sodium methallyl sulfonate to prepare modification liquid; and finally, modifying a polyamide fabric with the modification liquid to obtain the flame-retardant polyamide fabric. The initial limit oxygen index of the flame-retardant polyamide fabric prepared by the method reaches 35% or above, and belongs to the range of a nonflammable material; after 10 times of water washing, the limit oxygen index is not obviously reduced and still reaches 30% or above; and in addition, the flame retardance of the flame-retardant polyamide fabric prepared by the method exceeds that of a purchased flame-retardant polyamide fabric.

Description

technical field [0001] The invention belongs to the technical field of fabric preparation, and in particular relates to a flame-retardant nylon fabric and a preparation method thereof. Background technique [0002] With the continuous development of new textile materials and new technologies, the types of textiles are increasing day by day, and people's demand for functional textiles is also increasing. Flame-retardant textiles, as an umbrella to protect personal and property safety, have attracted more attention from people and achieved rapid development. . [0003] Nylon is a synthetic fiber that can be produced industrially. It has excellent physical properties and textile properties. It is resistant to wear, oil, low temperature, chemicals and deformation. It also has excellent tensile, impact and properties of flexural strength. In addition, nylon fiber is easy to dye, has high strength and good elasticity, so the fabrics made of it are widely used in production and l...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

Application Information

Patent Timeline
no application Login to View More
IPC IPC(8): D06M15/643D06M15/285D06M15/263D06M15/356C08F290/14C08F220/58C08F220/06C08F228/02C08G77/388D06M101/34
CPCD06M15/643D06M15/285D06M15/263D06M15/3566C08G77/045C08G77/388C08F290/148D06M2101/34D06M2200/30C08F220/585C08F220/06C08F228/02Y02E60/10
Inventor 周凡雨彭雄义崔永明董雄伟李强蔡亚君刘仰硕董会杰
Owner WUHAN TEXTILE UNIV
Who we serve
  • R&D Engineer
  • R&D Manager
  • IP Professional
Why Patsnap Eureka
  • Industry Leading Data Capabilities
  • Powerful AI technology
  • Patent DNA Extraction
Social media
Patsnap Eureka Blog
Learn More
PatSnap group products

Browse by: Latest US Patents, China's latest patents, Technical Efficacy Thesaurus, Application Domain, Technology Topic, Popular Technical Reports.

© 2024 PatSnap. All rights reserved.Legal|Privacy policy|Modern Slavery Act Transparency Statement|Sitemap|About US| Contact US: help@patsnap.com