Epoxy powder for packaging medium-low-voltage bus bar
A technology of epoxy powder and low-voltage busbar, which is applied in the field of packaging materials, can solve the problems of not being able to meet environmental protection and flame retardancy at the same time, unfavorable cost saving, long curing time, etc., achieve fluidized state effect and excellent durability of use, and filler Reasonable particle size matching and short curing time
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[0037] The method for synthesizing the phosphorus-containing silicon-containing polyurethane epoxy resin includes the following steps: firstly use a reactive phosphorus compound and an organic silicon resin to react with an isocyanate to obtain a phosphorus-containing silicon-containing polyurethane prepolymer with an isocyanate end group , And then use the reaction of isocyanate and epoxy resin to introduce the prepolymer into the molecular chain of epoxy resin to obtain a polyurethane epoxy resin containing phosphorus and silicon at the same time.
[0038] It includes the following steps:
[0039] (1) Under the protection of nitrogen, add isocyanate and catalyst to the reactor with heating device, stirrer and thermometer, heat up to 50~150℃, stir to make isocyanate and catalyst mix uniformly;
[0040] (2) Under stirring, slowly add the reactive phosphorus-containing compound to the reaction kettle in (1), and keep it warm for 1~8h;
[0041] (3) After the above reaction is over, slow...
Example Embodiment
[0109] Example 1
[0110] (1) First crush the raw materials to be crushed with a crusher;
[0111] (2) The raw materials are baked and dried separately, and then set aside;
[0112] (3) Weigh the filler and coupling agent according to the weight in Table 1, 25 kg of silica powder DRG800, 0.5 kg of coupling agent SG-TPT, put them into a stainless steel mixer and mix vigorously for 10 minutes, then surface modification of the filler;
[0113] (4) Combination of phosphorus-containing silicon-containing polyurethane epoxy resin A 40kg, curing agent KD402 20kg, toughening agent MBS 2.5kg, flame retardant aluminum hydroxide 0.5 kg, curing accelerator triphenylphosphine and imidazole 0.5kg, leveling agent GLP503 0.5kg, anti-scratch agent carnauba wax 0.5kg, pigment phthalocyanine blue 0.5kg, weighed according to the amount, put into a stainless steel mixer, and mixed vigorously for 10 minutes until uniform;
[0114] (5) Melt, knead and extrude the mixed raw materials with a screw extruder at ...
Example Embodiment
[0117] Example 2
[0118] The epoxy powder was prepared according to the steps described in Example 1, the components and their added amounts are shown in Table 1, and the inspection performance of the product is shown in Table 2.
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