Method for determining concentration of imidafenacin in blood plasma by liquid chromatography-mass spectrometry
A midanacin, LC/MS technology, applied in the field of medicine, can solve the problems of speed, precision, sensitivity, selectivity, etc. to be improved, and achieve the effect of high sensitivity, strong specificity, and stable baseline
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[0032] Example: Human K 2 Determination of Midanacin Concentration in EDTA Plasma
[0033] 1. Experimental materials and analytical equipment Midanacin (analyte): TLC Pharmaceutical Standards or the same or higher standard product Midanacin-d10 (internal standard): TLC Pharmaceutical Standards or the same or higher standard The reagents used in the product are shown in Table 1 below:
[0034] Table 1 Reagent Details
[0035] Reagent name level manufacturer Acetonitrile (ACN) HPLC J. T. Baker Ammonium acetate (CH 3 COONH 4 )
HPLC J. T. Baker Formic acid (FA) ACS Adamas Methanol (MeOH) HPLC J. T. Baker
[0036] Note: Reagents of the same grade or higher can also be used
[0037] The analytical equipment used is shown in Table 2 below:
[0038] Table 2 Details of equipment used
[0039]
[0040]
[0041] The same LC / MS / MS system can also be used.
[0042] 2. Liquid conditions
[0043] 1. Liquid chromatograph...
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