Online collection ionization device and method for cigarette smoke

A cigarette smoke and cigarette technology are applied in the field of cigarette smoke online collection and ionization devices, which can solve the problem of affecting the accuracy of smoking machine suction capacity, affecting the stability of mass spectrometry injection volume, and inability to take into account the accuracy of smoking capacity and smoke mass spectrometry Analyze quantitative accuracy and other issues to achieve the effect of strong device versatility, ensuring accuracy and stability, and ensuring stability

Pending Publication Date: 2021-05-28
ZHENGZHOU TOBACCO RES INST OF CNTC
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Problems solved by technology

Although the above two patents realize the online analysis of cigarette smoke, they cannot take into account the accuracy of the smoking capacity of the smoking machine and the quantitative accuracy of the mass spectrometry analysis of the smoke. The reason is that the mass spectrometer has its own vacuum system, whether through the quartz There is a constant suction flow in the capillary, through the flue gas collection bottle, and in the mass spectrometry system.

Method used

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  • Online collection ionization device and method for cigarette smoke
  • Online collection ionization device and method for cigarette smoke
  • Online collection ionization device and method for cigarette smoke

Examples

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[0042]Example

[0043]Such asimage 3 As shown, the ionization module 8 is provided as an electrospray ionization device including a sheath housing 81, and the sheath housing 81 is provided with a sheath gas inlet 83, and the line-in-chip cap 82 is disposed inside the sheath air shell 81. On the other end, the solvent 84 is connected, and the voltage 85 (preferably 3 to 5 kV) is applied to the quartz capillary 82, and the sheath housing 81 seals the vaporization chamber 7. The sphericular (preferably nitrogen) is accessed from the essence inlet 83 at a certain flow. The ionizing chamber condensed liquid discharge port can be set to switch the valve according to the actual needs to control the opening and closing of the switching valve.

[0044]Figure 4 It is shown that a continuous monitoring graph of glycerol and nicotine as the suction process in the suction process is released by a cigarette smoke online acquisition ionization device. Among them, the suction volume is 55ml, the suction ...

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Abstract

The invention discloses an online collection ionization device and method for cigarette smoke. The online collection ionization device for cigarette smoke comprises a cigarette holder, a suction module, a suction gas path, a sampling gas path, an ionization cavity and an ionization module, the cigarette holder is communicated with the suction module through the suction gas path, and the sampling gas path is communicated with the suction gas path, and the ionization module is communicated with the sampling gas path through the ionization cavity. According to the invention, online collection of fresh flue gas is realized; smoke collection and ionization processes are organically fused and simultaneously carried out, so that a powerful tool is provided for real-time online analysis of cigarette smoke; through the design of a plurality of components between the suction gas path and the sampling gas path, the suction capacity of the suction module is not influenced while smoke is collected, the accuracy and stability of puff-by-puff suction can be ensured, and the sample introduction and ionization stability of the ionization cavity can be ensured; the device is high in universality and can be adapted to various instruments or equipment for separation analysis based on the ionic state.

Description

Technical field[0001]The present invention relates to the field of cigarette flue gas analysis, in particular a cigarette smoke online acquisition ionization device and method.Background technique[0002]Collotable smoke as consumer's most direct object, its quality is an important factor in determining the quality of cigarettes. Strengthening cigarette smoke analysis, not only analyzing the quality of cigarettes, but also has important significance for guiding cigarette process formulations, processing and research and development.[0003]At present, the standard analysis method of cigarette flue gas analysis is based on off-line analysis, and the specific implementation is usually: collecting the particle portion of the cigarette smoke and the gas phase portion, respectively, by a certain sample. The pretreatment means obtains a suitable analysis test solution, and finally via conventional analysis techniques such as GC, LC, GC-MS, LC-MS. The formation of cigarette smoke is a dynamic ...

Claims

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Application Information

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IPC IPC(8): G01N27/62G01N1/24G01N1/28
CPCG01N27/62G01N1/24G01N1/28
Inventor 张齐张柯付丽丽徐波孙悦胡瑞林郭恒李斌王兵
Owner ZHENGZHOU TOBACCO RES INST OF CNTC
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