Organic electroluminescent device containing light extraction layer material
A technology of electroluminescent devices and light extraction layers, applied to organic compounds and their applications in organic electroluminescent devices, in the field of organic electroluminescent devices containing light extraction layer materials, can solve the problem of high evaporation temperature of inorganic materials, Slow evaporation rate and other issues, to achieve the effect of improving light extraction efficiency, high refractive index, and avoiding adverse effects
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[0203] The synthesis method of the compound according to the present invention is exemplified, but the present invention is not limited to the following examples.
[0204]
[0205] Synthesis of compound C-1:
[0206]
[0207] Compound 1-1 (4.86g, 15mmol), 1-2 (8.16g, 30mmol), potassium carbonate (6.26g, 45mmol), tetrakis (triphenylphosphine) palladium (0.52g, 0.45mmol) were placed in toluene In a three-necked flask with methanol (volume ratio 3:1), nitrogen was replaced three times, and the temperature was gradually raised to 80°C, and the reaction was stirred. After the TLC plate reactants disappeared, remove the heat source. After the system was cooled, water was added, the organic layer was separated, extracted three times with ethyl acetate, concentrated under reduced pressure, and passed through a silica gel column to obtain 4.19 g of compound I-3 with a yield of 45%.
[0208] Compound 1-3 (3.73g, 6mmol) was dissolved in anhydrous toluene, and 1-4 (0.92g, 6mmol), ...
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