Polyolefin composite microporous membrane and preparation method thereof
A microporous film and polyolefin technology, applied in the field of microporous film, can solve the problems of inability to guarantee the structural strength of the film, reduce product quality, film star microporous permeability and density, etc., to facilitate production and improve product quality. , to avoid the effect of cracking and breaking
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[0027] This preparation method comprises the steps:
[0028] P1. Weigh the raw materials respectively according to the mass percentage, and set aside;
[0029] P2. Put the polyolefin base material, additives and nanoparticles into the mixer, stir and mix evenly to obtain mixed raw materials;
[0030] P3. Put the mixed raw material into the melting equipment and heat it to 220°C to 260°C to form the molten raw material;
[0031] P4. Pass the molten raw material into the tape casting machine, and use a matte roller for casting traction to obtain a polyolefin base film;
[0032] P5. Heat-treating the polyolefin base film in fluorine gas with a concentration of 0.05%-0.08% at 110°C to 130°C for 20 to 30 seconds to obtain a heat-treated base film;
[0033] P6. The heat-treated base film is stretched and formed by a stretching machine under the condition of 100 degrees Celsius to 120 degrees Celsius to obtain a stretched base film;
[0034] P7. After the stretched base film is co...
Embodiment 1
[0046] A polyolefin composite microporous membrane and a preparation method thereof, wherein the microporous membrane comprises 79% of a polyolefin substrate, 15% of a treatment solution, 3% of nanoparticles and 3% of additives;
[0047] This preparation method comprises the steps:
[0048] P1. Weigh the raw materials respectively according to the mass percentage, and set aside;
[0049] P2. Put the polyolefin base material, additives and nanoparticles into the mixer, stir and mix evenly to obtain mixed raw materials;
[0050] P3. Put the mixed raw material into the melting equipment and heat it to 220°C to 260°C to form the molten raw material;
[0051] P4. Pass the molten raw material into the tape casting machine, and use a matte roller for casting traction to obtain a polyolefin base film;
[0052] P5. Heat-treating the polyolefin base film in fluorine gas with a concentration of 0.05%-0.08% at 110°C to 130°C for 20 to 30 seconds to obtain a heat-treated base film;
[0...
Embodiment 2
[0065] A polyolefin composite microporous membrane and a preparation method thereof, the microporous membrane comprising 77% of a polyolefin substrate, 15% of a treatment solution, 4% of nanoparticles and 4% of additives;
[0066] The preparation method comprises the steps of:
[0067] P1. Weigh the raw materials respectively according to the mass percentage, and set aside;
[0068] P2. Put the polyolefin base material, additives and nanoparticles into the mixer, stir and mix evenly to obtain mixed raw materials;
[0069] P3. Put the mixed raw material into the melting equipment and heat it to 220°C to 260°C to form the molten raw material;
[0070] P4. Pass the molten raw material into the tape casting machine, and use a matte roller for casting traction to obtain a polyolefin base film;
[0071] P5. Heat-treating the polyolefin base film in fluorine gas with a concentration of 0.05%-0.08% at 110°C to 130°C for 20 to 30 seconds to obtain a heat-treated base film;
[0072] ...
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