A medium-high temperature nanocomposite metal phase change heat storage material and its preparation method

A heat storage material and nano-composite technology, applied in the direction of heat exchange materials, metal processing equipment, chemical instruments and methods, etc., can solve the problems of low sensible heat density, environmental pollution, complex preparation process, etc.

Active Publication Date: 2021-08-20
CHINA UNIV OF MINING & TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

At present, the use of metals or alloys to prepare phase change materials mainly has problems such as low sensible heat density, difficulty in preventing leakage, complicated preparation process, high production cost, and serious environmental pollution; The material is prone to high-temperature reactions, so it is necessary to find a container with good compatibility with the metal

Method used

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  • A medium-high temperature nanocomposite metal phase change heat storage material and its preparation method
  • A medium-high temperature nanocomposite metal phase change heat storage material and its preparation method
  • A medium-high temperature nanocomposite metal phase change heat storage material and its preparation method

Examples

Experimental program
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Effect test

Embodiment 1

[0030] Such as figure 1 As shown, a method for preparing a medium-high temperature nanocomposite metal phase-change heat storage material, comprising the following steps:

[0031] (1) Put nano-copper powder with a particle size of 50nm and ordinary tin powder with a particle size of 74 μm into an ultrasonic disperser for 60 minutes;

[0032] (2) Put the nano-copper powder and ordinary tin powder into the ball mill respectively, the mass ratio between the nano-copper powder and the ordinary tin powder is 1:1; the ball mill first ball mills at a speed of 200r / min for 60min, and then at 100r / min Speed ​​ball milling for 60min, after mixing uniformly, copper-tin mixed particles were obtained;

[0033] (3) Compressing the copper-tin mixed particles with a pressure of 136 MPa by cold pressing method to obtain the first product of copper-tin composite phase change thermal storage material;

[0034] (4) Put the primary product of copper-tin composite phase change heat storage materi...

Embodiment 2

[0037] Such as figure 1 As shown, a method for preparing a medium-high temperature nanocomposite metal phase-change heat storage material, comprising the following steps:

[0038] (1) Put the nano-copper powder with a particle size of 50nm and the ordinary tin powder with a particle size of 74 μm into an ultrasonic disperser for 50 minutes;

[0039] (2) Put the nano-copper powder and ordinary tin powder into the ball mill respectively, the mass ratio between the nano-copper powder and the ordinary tin powder is 1:4; the ball mill first ball mills at a speed of 100r / min for 70min, and then at 150r / min Speed ​​ball milling for 50min, mixed uniformly to obtain copper-tin mixed particles;

[0040] (3) Compressing the copper-tin mixed particles with a pressure of 100 MPa by cold pressing method to obtain the first product of the copper-tin composite phase change thermal storage material;

[0041] (4) Put the primary product of copper-tin composite phase change heat storage materi...

Embodiment 3

[0044] Such as figure 1 As shown, a method for preparing a medium-high temperature nanocomposite metal phase-change heat storage material, comprising the following steps:

[0045] (1) Put nano-copper powder with a particle size of 50nm and ordinary tin powder with a particle size of 74 μm into an ultrasonic disperser for 70 minutes;

[0046] (2) Put the nano-copper powder and ordinary tin powder into the ball mill respectively. The mass ratio between the nano-copper powder and the ordinary tin powder is 3:7; the ball mill first ball mills at a speed of 300r / min for 50min, and then at 50r / min Speed ​​ball milling for 70min, mixed uniformly to obtain copper-tin mixed particles;

[0047] (3) Compressing the copper-tin mixed particles with a pressure of 500 MPa by cold pressing method to obtain the first product of the copper-tin composite phase change thermal storage material;

[0048] (4) Put the primary product of copper-tin composite phase change heat storage material into a...

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Abstract

A method for preparing a medium-high temperature nano-composite metal phase-change heat storage material, comprising the following steps: respectively putting nano-copper powder with a particle size of 50 nm and ordinary tin powder with a particle size of 74 μm in an ultrasonic disperser for 50-70 minutes; Put into a ball mill and mix evenly to obtain copper-tin mixed particles; the mass ratio between nano-copper powder and ordinary tin powder is 1: (1-9); the copper-tin mixed particles are pressed into shape with a pressure of 100-500MPa by cold pressing method, The primary product of the copper-tin composite phase change thermal storage material is obtained; the primary product of the copper-tin composite phase change thermal storage material is put into a tube furnace for sintering at a sintering temperature of 250-300°C, kept for 30-40 minutes, and then naturally cooled to room temperature. Finally, a medium-high temperature copper-tin composite phase change heat storage material is obtained. The method can simplify the production process, reduce the production cost and reduce the pollution to the environment, and the prepared material can have high heat storage density, high thermal conductivity, excellent leakage resistance and excellent mechanical properties.

Description

technical field [0001] The invention relates to the technical field of phase change materials, in particular to a medium-high temperature nanocomposite metal phase change heat storage material and a preparation method thereof. Background technique [0002] Phase change heat storage material refers to a substance that is accompanied by a large amount of heat absorption or heat release when a solid-liquid phase change occurs at a specific temperature (ie, phase change temperature). Nearly isothermal and other characteristics, it is widely used in the field of heat flux adjustment and temperature control, so as to realize peak shifting and valley filling of heat flux and improve energy utilization efficiency. [0003] According to the classification of phase change materials, it can be divided into organic phase change materials, inorganic phase change materials and composite phase change materials. In practical applications, phase change materials are usually classified accor...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C09K5/06B22F1/00B22F3/02B22F3/10B22F9/04
CPCC09K5/063B22F9/04B22F3/02B22F3/10B22F2009/043B22F1/052Y02E60/14
Inventor 黄丛亮蓝迎莹
Owner CHINA UNIV OF MINING & TECH
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