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Alkaloid and phenol reaction composition, atomized liquid, atomization bomb and electronic atomizer

An electronic atomizer and alkaloid technology, which is applied in the fields of atomizing bombs, electronic atomizers, atomizing liquid, alkaloid and phenol reaction compound, which can solve the problem of weak roar, slow e-cigarette addiction relief, and vaping problems. Poor absorption experience and other problems, to achieve the effect of facilitating the entrance and improving the irritating taste of the throat

Pending Publication Date: 2021-07-13
ZHANGJIAGANG ALIEN NEW MATERIAL TECH CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Free nicotine is volatile, unstable, irritating, and choking, and organic acid nicotine salt enters the human body during atomization, causing problems such as "acidosis", "excess acid" and "sour smell"
[0005] In addition, in order to reduce the dependence of nicotine addiction, reducing the concentration of nicotine in the atomized liquid has become a global policy and regulation trend; The competitiveness of e-cigarettes and traditional tobacco will be reduced, which will lead users to choose traditional tobacco again

Method used

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  • Alkaloid and phenol reaction composition, atomized liquid, atomization bomb and electronic atomizer
  • Alkaloid and phenol reaction composition, atomized liquid, atomization bomb and electronic atomizer
  • Alkaloid and phenol reaction composition, atomized liquid, atomization bomb and electronic atomizer

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0071] In a polytetrafluoroethylene plastic container, add 95.16 grams of propylene glycol as the reaction medium, and add 1.63 grams of plant-extracted nicotine liquid with a purity of 99.5% (C 10 h 14 N 2 , the number of N atoms is about 0.02 moles) and 3.21 grams of cannabidiol powder with a purity of 98% (C 21 h 30 o 2 , about 0.02 moles of phenolic hydroxyl) as the reactant, moles of alkaloid nitrogen atoms / moles of phenolic hydroxyl = 1 / 1, seal the polytetrafluoroethylene container into a hydrothermal reaction kettle and put it into a circular sleeve for temperature control and magnetic stirring In the container, turn on the heating, set a continuous stirring speed of 300rps and heat at a constant temperature of 150°C for 120 minutes, turn off the power and cool naturally, then take out the polytetrafluoroethylene container to obtain the nicotine-cannabidiol reaction containing the bound "alkaloid-phenol" A mixture of synthetics and propylene glycol, in which nicotin...

Embodiment 2

[0075] In the three-neck round bottom flask, add 150.53 grams of propylene glycol as the reaction medium, and add 4.87 grams of artificial nicotine liquid with a purity of 99.9% (C 10 h 14 N 2 , the number of N atoms is about 0.06 moles), 1.58 grams of arecoline with a purity of 98% (C 8 h 13 NO 2 , the number of N atoms is about 0.01 moles), 3.19 grams of cannabigerol powder with a purity of 99% (C 21 h 32 o 2 , about 0.02 moles of phenolic hydroxyl groups), moles of nitrogen atoms in alkaloids / moles of phenolic hydroxyl groups = 3.5 / 1, use a round heater to control the reaction temperature in the round bottom flask to 40°C, continue heating and stirring for 6000 minutes, then turn off the power Cool naturally to obtain a mixture of (nicotine + arecoline)-cannabigerol reaction composition and propylene glycol containing the bound "alkaloid-phenol", add 1 gram of sucralose sweetener and 1 gram of menthol to cool Flavor essence, marked as "B2 atomized liquid", in which ...

Embodiment 3

[0078] In the polytetrafluoroethylene container, add 29.74 grams of propylene glycol and 1 gram of water as the reaction mixed medium, add 0.0181 grams of theophylline powder (C 7 h 8 N 4 o 2 , the number of N atoms is about 0.0004 moles), 316.24 grams of carvacrol liquid with a purity of 95% (C 10 h 14 O, about 2 moles of phenolic hydroxyl groups) and 267.62 grams of chrysophanol powder with a purity of 95% (C 15 h 10 o 4 , about 2 moles of phenolic hydroxyl groups) as reactants, moles of alkaloid nitrogen atoms / moles of phenolic hydroxyl groups=0.0001 / 1, seal the polytetrafluoroethylene container into a hydrothermal reactor, close the reactor and put it into In the temperature-controlled magnetic stirrer, turn on the heating, set the continuous stirring speed to 300rps and heat at a constant temperature of 130°C for 20 minutes, turn off the power and cool naturally, then take out the polytetrafluoroethylene container to obtain the theophylline-( Carvacrol + chrysophan...

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Abstract

The invention discloses an alkaloid and phenol reaction composition, atomized liquid, an atomization bomb and an electronic atomizer. The alkaloid and phenol reaction composition comprises a composition R-PH-O-N-I obtained by chemical reaction of alkaloid and phenol, the general formula of the chemical reaction is R-PH-OH + N-I = = R-PH-O-N-I. A reactant alkaloid and a reactant phenol are added into a reaction container, heating is performed, and heating and stirring are continuously performed at 40-300 DEG C for 0.1-6000 minutes to obtain the alkaloid and phenol reaction composition. Through the mode, according to the alkaloid and phenol reaction composition, the atomized liquid and the atomized bomb, the problems that in an electronic atomizer, alkaloid originally chokes the throat and has stimulation smell are solved, the alkaloid and phenol reaction composition is beneficial to the mouth and cannot cause acidosis, excessive acid, sour odor and the like, and faster, more pleasant and satisfied smoking experience can be obtained.

Description

technical field [0001] The invention relates to the fields of organic chemical synthesis and electronic atomization, in particular to an alkaloid-phenol reaction compound, an atomizing liquid, an atomizing bomb and an electronic atomizer. Background technique [0002] Electronic atomizers, also known as electronic cigarettes, are effective tools to help smokers quit smoking. They are mainly divided into vapor electronic atomizers (Vapor) that consume liquid atomizing bombs and heat-not-burn electronic atomizers that consume solid atomizing bombs. Device (HNB) two categories. Compared with traditional tobacco, these two types of e-cigarettes can efficiently transmit nicotine, and can greatly reduce the entry of tar, carbon monoxide, nitric oxide and other harmful substances into the human body, so they have been used by hundreds of millions of users around the world as "harm reduction products". [0003] However, research on the hazards of e-cigarettes is not thorough. For ...

Claims

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Application Information

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IPC IPC(8): A24F40/42A24F40/10A24F40/40A24B15/167
CPCA24F40/42A24F40/10A24F40/40A24B15/167
Inventor 冯婷
Owner ZHANGJIAGANG ALIEN NEW MATERIAL TECH CO LTD
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