Preparation method of antibacterial coating

A technology of antibacterial coatings and antibacterial agents, applied in the field of preparation of antibacterial coatings, can solve the problems of antibacterial properties, scrub resistance, alkali resistance, water resistance and artificial aging resistance, and complex preparation methods. , to achieve the effects of easy operation, strong adhesion and strong resistance to artificial aging

Inactive Publication Date: 2021-07-16
CYPRESS BIO TECH CO LTD +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0002] Paint is sprayed or brushed on the surface of the building or decoration to be coated, and can form a continuous film with the surface of the object to be coated. There are many types of paint, including water-based paint, latex paint, etc. After the film is formed, there are various formula ratios for antibacterial properties, scrub resistance, water resistance and artificial aging resistance. At present, most of the preparation methods of antibacterial coatings use relatively complex ingredients, and the preparation methods are complicated. And in Antibacterial, scrub resistance, alkali resistance, water resistance and artificial aging resistance can not be better

Method used

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  • Preparation method of antibacterial coating
  • Preparation method of antibacterial coating

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0025] 1) Will Evonik SIVO 160 silane coupling agent 40 parts, Evonik 10 parts of SIVO110 coupling agent, 18 parts of antibacterial agent dimethyl octadecyl [3-(trimethoxysilyl) propyl] ammonium chloride, 100 parts of adhesive acrylic acid and 200 parts of organic solvent ethanol were added in turn The polymer is obtained in the reactor, and the above parts are parts by weight.

[0026] SIVO 160 is an aqueous silane sol-gel system, in the form of colorless to light yellow, low viscosity liquid, SIVO 110 is a water-based silane sol-gel system, opaque to emulsion, color from colorless to light yellow.

[0027] 2) Drop deionized water or distilled water that is 632 parts by weight into the polymer of step (1), and stir at 150 rpm to obtain an antibacterial coating;

[0028] 3) Stir the antibacterial coating obtained in step 2) for 2 hours at a speed of 30 rpm, then transfer it to a sealed container and let it stand for 12 hours.

Embodiment 2

[0030] 1) 223 parts of silane coupling agent methyltrimethoxysilane, 18 parts of antibacterial agent dimethyloctadecyl [3-(trimethoxysilyl) propyl] ammonium chloride, 83 parts of adhesive acrylic acid 30 parts of crosslinking agent triethoxyvinyl silane and 92 parts of organic solvent ethanol were respectively added into the reaction kettle to obtain a polymer, and the above parts are parts by weight.

[0031] 2) Drop deionized water or distilled water that is 554 parts by weight into the polymer in step (1), and stir at 180 rpm to obtain an antibacterial coating;

[0032] 3) Stir the antibacterial coating obtained in step 2) for 2 hours at a speed of 35 rpm, then transfer it to a sealed container and let it stand for 12 hours.

Embodiment 3

[0034] 1) Add 218 parts of silane coupling agent methyltrimethoxysilane, 15 parts of 3-(2,3-epoxypropoxy)propyltrimethoxysilane, 14 parts of (2-cyanoethyl)triethoxysilane 16 parts, 16 parts of antibacterial agent dimethyloctadecyl [3-(trimethoxysilyl) propyl] ammonium chloride, 91 parts of adhesive acrylic acid and 91 parts of organic solvent ethanol are respectively added in the reactor to obtain polymerization The above parts are parts by weight.

[0035] 2) Drop deionized water or distilled water with 555 parts by weight into the polymer of step (1), and stir at 200 rpm to obtain antibacterial coating;

[0036] 3) Stir the antibacterial coating obtained in step 2) for 2 hours at a speed of 30 rpm, then transfer it to a sealed container and let it stand for 12 hours.

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Abstract

The invention provides a preparation method of an antibacterial coating. The preparation method comprises the following steps: (1) sequentially and respectively adding a silane coupling agent, an adhesive, an antibacterial agent and an organic solvent into a reaction kettle to obtain a polymer, wherein the weight part ratio of the silane coupling agent to the adhesive to the antibacterial agent to the organic solvent is (1-348): (2-250): (3-120): (16-340); (2) dropwise adding 200-980 parts by weight of deionized water or distilled water into the polymer in the step (1), and stirring at the rotating speed of 100-300rpm while dropwise adding to obtain the antibacterial coating; (3) stirring the antibacterial coating obtained in the step (2) at the rotating speed of 20-50rpm for 2 hours, transferring into a sealed container, and standing for more than 12 hours; the preparation method has the beneficial effects that the sprayed coating has a long-acting antibacterial effect and has relatively high alkali resistance, water resistance and artificial aging resistance.

Description

technical field [0001] The invention relates to the technical field of paint chemical industry, in particular to a preparation method and application of an antibacterial paint. The product has long-acting antibacterial effect and has high alkali resistance, water resistance and artificial aging resistance. Background technique [0002] Paint is sprayed or brushed on the surface of the building or decoration to be coated, and can form a continuous film with the surface of the object to be coated. There are many types of paint, including water-based paint, latex paint, etc. After the film is formed, there are various formula ratios for antibacterial properties, scrub resistance, water resistance and artificial aging resistance. At present, most of the preparation methods of antibacterial coatings use relatively complex ingredients, and the preparation methods are complicated. And in Antibacterial, scrub resistance, alkali resistance, water resistance and artificial aging resis...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C09D4/02C09D5/14
CPCC09D4/00C09D5/14
Inventor 蔡峥鸣潘伯恒
Owner CYPRESS BIO TECH CO LTD
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