Anode materials, electrochemical devices and electronic devices
A negative electrode material, electrochemical technology, applied in the field of electrochemistry, can solve problems such as unsatisfactory, and achieve the effect of improving cycle performance
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[0044] In some embodiments of the present application, a method for preparing an electrochemical device is also proposed, comprising the following steps:
[0045] Preparation of negative electrode material:
[0046] Step 1: 500g of amorphous silicon oxide powder with a particle size of 1mm to 100mm and a chemical formula of SiOx (0.5≤x≤1.6) is first subjected to mechanical crushing treatment, and then air crushed with a jet mill, and then classified to obtain the particle size Silica powder in the range of 0.2 μm to 30 μm.
[0047] Step 2: Place the silicon oxide powder obtained in Step 1 in a CVD (Chemical Vapor Deposition, Chemical VaporDeposition) furnace, heat up to 900°C to 1000°C, fill with a carbon source gas, and the gas flow rate is 300mL / min. After 60min Cut off the carbon source gas immediately. It was warmed to room temperature under an inert atmosphere, and the powder samples were taken out after cooling. Inert atmosphere is Ar, N 2 , one or more mixtures of H...
Embodiment 1
[0060] Preparation of negative electrode material:
[0061] Step (1): The particle size of 500g is 1mm to 100mm, and the chemical formula is SiO x The amorphous silicon oxide powder (0.5≤x≤1.6) is first subjected to mechanical crushing, and then air crushed with a jet mill to obtain silicon oxide powder with a particle size range of 0.2μm to 30μm. SiO x .
[0062] Step (2): the SiO obtained in step (1) x It was placed in a CVD furnace, heated to 960°C, filled with methane, the gas flow was 300mL / min, and the methane gas was cut off immediately after maintaining for 120min. The temperature was lowered to room temperature in an inert Ar atmosphere, and the carbon-coated silicon-oxygen material was taken out after cooling.
[0063] Step (3): perform demagnetization treatment, classification treatment, and 1300-mesh sieve on the carbon-coated silicon-oxygen material obtained in step (2) to obtain a carbon-coated silicon oxide negative electrode material.
[0064] Preparation ...
Embodiment 2
[0073] The only difference between Example 2 and Example 1 is that in step (3) of preparing the negative electrode material, a 1200-mesh screen is used for sieving, which is the same as Example 1.
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