Application of organic solvent-resistant nanofiltration membrane in capsorubin pungency removal
A technology resistant to organic solvents and capsanthin, applied in organic chemistry, organic dyes, membrane technology, etc., can solve the problems of large solvent consumption, complex process, high cost, etc., achieve low processing temperature, simple process, and realize recycling Effect
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Embodiment 1
[0046] The present embodiment relates to a kind of despicy technology of capsanthin, comprises the steps:
[0047] 1) Put 500g of pepper granules (color value E16.3, spiciness 0.2%) into the extractor, add 5000ml of n-hexane, extract continuously at 45°C for 3.5 hours, extract by centrifugation at 4000rpm, and centrifuge for 5min to obtain 4500ml of pepper Extract filtrate, after testing, wherein the mass concentration of capsanthin is 7.42g / L;
[0048] 2) The filtrate enters the first-level organic solvent-resistant nanofiltration membrane, the temperature of the feed liquid is 30-35°C, the operating pressure of the membrane equipment is 1.6-2.1MPa, and the separation operation is performed to obtain a primary retentate and a primary permeate; the retentate is scraped After removing the remaining solvent by evaporating the plate film, 31.88g of capsanthin and 300ml of solvent were obtained. The unit color value of capsanthin was E251.3, and the spiciness was 0.001%. 99.97%, ...
Embodiment 2
[0051] The present embodiment relates to a kind of despicy technology of capsanthin, comprises the steps:
[0052]1) Put 500g of capsicum granules (color value E16.3, spiciness 0.2%) into the extractor, add 5000ml of acetone, and extract continuously at 45°C for 3.5 hours. The extract is centrifuged at 4000rpm and centrifuged for 5min to obtain 4500ml of capsicum extract Filtrate, after testing, wherein the mass concentration of capsanthin is 7.39g / L;
[0053] 2) The filtrate enters the first-level organic solvent-resistant nanofiltration membrane, the temperature of the feed liquid is 30-35°C, the operating pressure of the membrane equipment is 1.6-2.1MPa, and the separation operation is carried out to obtain the first-level retentate and the first-level permeate; the retentate After the remaining solvent was removed by scraper film evaporation, 31.95g of capsanthin and 800ml of solvent were obtained. The unit color value of capsanthin was E248.8, and the spiciness was 0.003%...
Embodiment 3
[0056] The present embodiment relates to a kind of despicy technology of capsanthin, comprises the steps:
[0057] 1) Put 500g of pepper granules (color value E16.3, spiciness 0.2%) into the extractor, add 5000ml of n-hexane, extract continuously at 45°C for 3.5 hours, extract by centrifugation at 4000rpm, and centrifuge for 5min to obtain 4500ml of pepper Extract filtrate, after testing, wherein the mass concentration of capsanthin is 7.39g / L;
[0058] 2) The filtrate enters the first-level organic solvent-resistant nanofiltration membrane, the temperature of the feed liquid is 35-38°C, the operating pressure of the membrane equipment is 1.8-2.1MPa, and the separation operation is carried out to obtain the first-level retentate and the first-level permeate; the retentate After the remaining solvent was removed by scraper film evaporation, 31.74g of capsanthin and 200ml of solvent were obtained. The unit color value of capsanthin was E252.7, and the spiciness was 0.0005%. The...
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