Heating cigarette cooling section containing layered perovskite and preparation method thereof
A technology of perovskite and cooling section, used in tobacco, cigarette manufacturing, e-liquid filter, etc., can solve the problems of poor smoking quality, strong thermal irritation of smoke, high water content in smoke, and achieve high latent heat of phase transition. , Easy to apply on a large scale, stable chemical properties
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[0026] The disclosure provides a method for preparing a cooling section of a heated cigarette containing layered perovskite, including the following steps:
[0027] Step (1): After dissolving the water-soluble polymer material, add layered perovskite, and stir evenly to obtain a mixed solution.
[0028] In order to improve the cooling efficiency, the mass ratio of the water-soluble polymer material and the layered perovskite in step (1) may be (5-7):(3-5).
[0029] In order to improve cooling efficiency, the water-soluble polymer material in step (1) may include at least one of polyvinyl alcohol, modified starch, hydroxypropyl cellulose, carboxymethyl cellulose and gelatin.
[0030] In order to improve cooling efficiency, the layered perovskite in step (1) can include (C 12 h 25 NH 3 ) 2 ZnCl 4 , (C 14 h 29 NH 3 ) 2 ZnCl 4 , (C 16 h 33 NH 3 ) 2 ZnCl 4 , (C 12 h 25 NH 3 ) 2 CoCl 4 , (C 14 h 29 NH 3 ) 2 ZnCl 4 , (C 16 h 33 NH 3 ) 2 CoCl 4 , 0(C 12 ...
Embodiment 1
[0042] 1. Dissolve 50 parts of polyvinyl alcohol 1799 in water, then add 50 parts of (C 12 h 25 NH 3 ) 2 ZnCl 4 After the powder is stirred evenly, a mixed solution with a mass concentration of 20 wt% is formed. Among them, (C 12 h 25 NH 3 ) 2 ZnCl 4 The phase transition temperature is 88°C, and the latent heat of phase transition is 97J / g.
[0043] 2. Coat the mixed solution on the surface of cellulose paper and dry at 80°C to obtain a composite cooling material with a coating thickness of 5um.
[0044] 3. The composite cooling material is embossed, wrapped with paper material, and cut into sections to obtain the cooling section S1 of the heated cigarette, and the embossed width is 1 mm.
[0045] The cooling section S1 is applied to the heated cigarette. When the smoke passes through the cooling section, the temperature of the smoke is reduced by 43°C, the inlet smoke temperature is 46.3°C, and the moisture content of the smoke is reduced, which effectively improves...
Embodiment 2
[0047] 1. Dissolve 65 parts of polyvinyl alcohol 1799 in water, then add 35 parts of (C 16 h 33 NH 3 ) 2 ZnCl 4 After the powder is stirred evenly, a mixed solution with a mass concentration of 15 wt% is formed. Among them, (C 16 h 33 NH 3 ) 2 ZnCl 4 The phase transition temperature is 99°C, and the latent heat of phase transition is 117J / g.
[0048] 2. Coat the mixed solution on the surface of cellulose paper and dry at 75°C to obtain a composite cooling material with a coating thickness of 3.5um.
[0049] 3. Emboss the composite cooling material, gather and wrap it with paper material, and cut into sections to obtain the cooling section S2 of the heated cigarette. The width of the embossing treatment is 1.5 mm.
[0050] The cooling section S2 is applied to the heated cigarette. When the smoke passes through the cooling section, the temperature of the smoke is reduced by 45.6°C, the inlet smoke temperature is 48.2°C, and the moisture content of the smoke is reduced,...
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Abstract
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