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A kind of nickel-based alloy with nanostructure and γ` phase composite structure and preparation method thereof

A technology of nickel-based alloy and composite structure, which is applied in the field of nickel-based alloy with nanostructure and γ' phase composite structure and its preparation, can solve the problems of difficulty in regulation, treatment of uneven layer structure, sacrificial plasticity, etc., and achieves easy control. , easy to deform process parameters, improve the effect of strength

Active Publication Date: 2022-04-08
NANJING UNIV OF SCI & TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

However, it often brings disadvantages such as insufficient material deformation or difficult to control, and the improvement of strength must be at the expense of plasticity.
For example, technologies such as rolling, laser pulse shock, surface mechanical grinding treatment and surface mechanical rolling treatment have certain defects in the treatment methods, including low treatment efficiency, low energy utilization rate, uneven structure of the treatment layer and high surface roughness. This hinders the promotion and application of various metal materials to a certain extent

Method used

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  • A kind of nickel-based alloy with nanostructure and γ` phase composite structure and preparation method thereof
  • A kind of nickel-based alloy with nanostructure and γ` phase composite structure and preparation method thereof
  • A kind of nickel-based alloy with nanostructure and γ` phase composite structure and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0039] (1) The chemical element in the nickel-based alloy to be treated is measured as follows (at.%) As follows: Ni: 48.70%, CO: 22.94%, Cr: 15.46%, Al: 5.10%, Ti: 4.96%, MO: 1.81%, W: 0.34%, Fe: 0.51%, Zr: 0.02%, C: 0.11%, B: 0.05%;

[0040] The nickel-based alloy was carried out to give a nickel-based alloy containing a γ 'phase strengthening γ matrix structure.

[0041] (2) Treatment of nickel-based alloys containing γ 'phase strengthening γ matrix structure by surface mechanical rolling, defects in its surface layer.

[0042] (3) For the nickel-based alloy of step (2), the surface mechanical rolling treatment is continuously repeated, and the surface mechanical rolling treatment containing the total number of 3 is finally composite containing layer-containing dentist. The nickel-based alloy structure of the structure has a high strength with the γ 'phase composite structure.

[0043] The surface mechanical rolling treatment parameters are: the rod-shaped nickel-based alloy di...

Embodiment 2

[0046] Different from Example 1 in:

[0047] The tissue structure of the nickel-based alloy surface is obtained by the surface mechanical rolling treatment to refine the grain size γ 'phase structure, ie twin, layer error and γ' phase composite structure nickel base alloy. Layer error and twin crystal are high in strength. The chemical element in the nickel-based alloy is the same as in Example 1. The surface mechanical rolling treatment parameters are: the rod-shaped nickel-based alloy diameter is 11 mm, the rotational speed is 600 r / min, and the cutter head is 8 mm WC - Co hard alloy gold ball, which has a feed speed of 40 mm / min, each The hard alloy ball head in the process of treatment is 20 μm in the lower surface of the nickel-based alloy surface, and the processing path is 5. In this embodiment, the thickness of the nickel-based alloy surface of the present embodiment, the thickness of the layer is 130 μm, the γ 'phase composite structure is 30 Nm, and the nickel-based ...

Embodiment 3

[0049] Different from Example 1 in:

[0050] The tissue structure of the nickel-based alloy surface is obtained by laying the surface mechanical rolling treatment to refine the grain size γ 'phase structure, and the structure of the surface layer γ' phase is completely destroyed. A nickel-based alloy, nickel-based alloy, nanocrystalline, nanocrystalline, and layer dislocation, nanocrystalline, and layer dislocations, nanocrystalline, and layer dislocations, and γ 'phase composite structures having a large-scale grain size and gamma phase element enriched region average grain size. The chemical element in the nickel-based alloy is the same as in Example 1. The surface mechanical rolling treatment parameters are: the rod-shaped nickel-based alloy diameter is 11 mm, the rotational speed is 600 r / min, and the cutter head is 8 mm WC-Co hard With the golden ball, the feed rate is 40 mm / min, and the hard alloy ball head in each process is 20 μm in the lower depth of the nickel-based ...

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Abstract

The invention discloses a nickel-based alloy with a composite structure of nanostructure and γ' phase and a preparation method thereof, and relates to the technical field of nanostructure metal materials. The microstructure of the surface layer of the nickel-based alloy contains a γ' phase whose size is refined, and the defects are stacking faults, twins and nanocrystals, and the γ' phase is refined in different degrees. This method uses different passes of surface mechanical rolling to treat nickel-based alloys containing γ' phases successively, so as to prepare γ' phases with different degrees of refinement on the surface of nickel-based alloys, and the size distribution of the enriched regions of the γ' phase elements At 13-40 nm, the microhardness of the structure is between 5.4-6.8 GPa, which is 1.1-1.4 times that of the nickel-based alloy before surface treatment, which not only improves the strength of the nickel-based alloy as a whole, but also can obtain Nickel-based alloys with different strength requirements.

Description

Technical field [0001] The present invention relates to the field of nanostructured metal materials, and more particularly to a nickel-based alloy having a nanostructure and a γ 'phase composite structure and a preparation method thereof. Background technique [0002] Nickel-based alloys are widely used in aerospace engines, transportation, petrochemical and nuclear industries. The main phase structure present in the nickel-based alloy is γ phase, γ 'phase and carbide, etc. Strengthen, second phase strengthening, and grain boundary enhancement, but may result in changes in the physical and chemical properties of alloys. In addition, people also attempt to improve the strength of the alloy by introducing various defective structures in the alloy system, but it is difficult to avoid the plasticity and thermal stability of the alloy in the alloy. [0003] 文献Zhang HW, Huang X, Hansen N. Evolution of microstructuralparameters and flow stresses toward limits in nickel deformed to ultra...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C22F1/10C22C19/05C22C30/00
CPCC22F1/10C22C19/056C22C30/00
Inventor 张勇吴豪袁圣云姜智浩冯天
Owner NANJING UNIV OF SCI & TECH