Method for simultaneously producing five components in flaxseeds

A technology of linseed and linseed oil, which is applied in the preparation methods of peptides, chemical instruments and methods, fat oil/fat production, etc., can solve the problems of high cost, low separation efficiency, large consumption of ethanol, etc., and achieves reduction of interfering substances. , the effect of improving the production rate and improving the extraction rate

Pending Publication Date: 2021-10-22
天水雪陆鱼生物科技有限责任公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

With the development of society, some flaxseed kernel separation technologies have been developed in recent years. However, due to the high oil content in flaxseed kernels, some of these technologies are only in the laboratory research stage and cannot be applied industrially. Individually applied to actual production, but the high cost and low separation efficiency greatly restrict the large-scale application
Patent CN108686736B discloses "a method for separating linseed shell and kernel based on ethanol wet filtration". When the linseed is broken, the shell is indeed larger than the kernel, but a considerable part of the shell will also be broken into powder In addition, there will also be some linseeds that are not crushed so finely that they cannot pass through the sieve. Therefore, in the actual operation of this method, it is difficult to separate the husks completely, and linseed oil is slightly soluble in ethanol, not easily soluble in ethanol. , so this method consumes a lot of ethanol, has no practical application value, and cannot obtain relatively complete flaxseed kernels

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0022] (1) 50kg of linseed and hot water at 60°C were mixed and extracted for 1 hour, squeezed and filtered with gauze to obtain the filtrate and filtered linseed, filtered linseed was extracted 5 times according to the above method, and the extracts were combined to obtain Degummed flaxseed and filtrate A

[0023] (2) In the above step (1), roast the degummed flaxseed at 60°C to remove water until the moisture content is lower than 1.8%, and then use a hydraulic oil press to extract the oil at a temperature of 25°C and a pressure of 30MPa to obtain flaxseed oil A and defatted flaxseed; dehulling the defatted flaxseed with a sheller to obtain flax bark and flaxseed A;

[0024] (3) The flax bark obtained in the above step (2) is crushed and then mixed with sodium hydroxide solution at a ratio of 1:5, stirred and extracted at 80°C for 2 hours, filtered, extracted 5 times, and the extracts are combined, and the pH is adjusted to neutral , to obtain filtrate B and filter residue;...

Embodiment 2

[0032] (1) 200kg of selected linseeds and 20°C water were mixed and extracted at a ratio of 1:15 for 5 hours. After extraction, squeeze and filter with gauze to obtain filtrate and filter linseeds. Filter linseeds and extract 3 times according to the above method. Combine the extracts to obtain degummed linseed and filtrate A;

[0033] (2) The above-mentioned degummed linseeds are dried outdoors to remove water until the moisture content is lower than 1.8%, and then the oil is extracted with a hydraulic oil press at a temperature of 10°C and a pressure of 40 MPa to obtain linseed oil A and defatted linseeds; The degreased flaxseed is dehulled with a sheller to obtain flax bark and flaxseed A;

[0034] (3) The flax bark obtained in the above step (2) is crushed and then mixed with potassium hydroxide solution at a ratio of 1:10, stirred and extracted at 60°C for 3 hours, filtered, extracted 3 times, and the extracts are combined, and the pH is adjusted to neutral , to obtain f...

Embodiment 3

[0042] (1) Mix 500kg of selected flaxseeds with water at 95°C at a ratio of 1:3, stir and extract for 2 hours. After extraction, squeeze and filter with gauze to obtain the filtrate and filter residue. The filter residue is then extracted 8 times according to the above method, and the extracts are combined. Obtain degummed linseed and filtrate A;

[0043] (2) In the above step (1), the degummed flaxseeds are roasted at 50°C to remove water until the moisture content is lower than 1.8%, and then the oil is pressed by a hydraulic oil press at a temperature of 60°C and a pressure of 25MPa to obtain flaxseeds Oil A and defatted flaxseed; dehulling the defatted flaxseed with a sheller to obtain flax bark and flaxseed A;

[0044] (3) The flax bark obtained in the above step (2) is crushed and then mixed with sodium hydroxide solution at a ratio of 1:3, stirred and extracted at 90°C for 1 hour, filtered, extracted 8 times, and the extracts are combined, and the pH is adjusted to neut...

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PUM

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Abstract

The invention discloses a method for simultaneously producing five components in flaxseeds. The method comprises the following steps: (1) primarily extracting linseed gum and lignan from the flaxseeds; (2) performing cold pressing on the degummed linseeds by a hydraulic oil pressing machine to prepare linseed oil; (3) performing peel-kernel separation on the degummed and degreased flaxseeds; (4) crushing the flax peel subjected to peel-kernel separation, and extracting flax gum and secoisolariciresinol diglucoside again; (5) preparing flaxseed oil from the flaxseeds subjected to peel and kernel separation again; (6) extracting flax protein from the degreased flaxseed; (7) separating linseed cyclic peptide from the linseed oil prepared twice; and (8) extracting the flax cyclic peptide from the degreased and deproteinized flaxseed again. The steps are linked, the preliminary extraction or preparation of part of the components provides favorable conditions for the separation of the flax peel and kernel, the extraction or preparation rates of the components and other components are improved after the separation of the flax peel and kernel, the components supplement each other, the cost is low, the process is simple and easy to operate, the method is green and environment-friendly, and large-scale production can be realized; and the five components are produced at the same time, so that the additional value of the flaxseeds is greatly improved.

Description

technical field [0001] The invention relates to a method for simultaneously producing several components from linseed, in particular to a method for simultaneously producing five components such as linseed oil, linseed gum, linseed lignan, linseed protein and linseed cyclopeptide. Background technique [0002] Flax (Linum usitatissimum L.), also known as flax, is one of the seven major oil crops in the world. my country's flaxseed production is second only to Canada, ranking second in the world. Flaxseed contains a variety of valuable components, such as linseed gum, lignans, linseed oil, linseed cyclopeptide, flax protein, etc., while linseed gum and lignans mainly exist in the linseed bark, and flaxseed Oil, flaxcycline, and flax protein are mainly found in the flaxseed kernel. Linseed gum and lignans are directly extracted from non-peeled flax seeds. Since the flax bark is not broken, the extraction rate of flaxseed gum and lignans is low, and there are still high residu...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C07H15/18C07H1/08C11B1/04C11B1/06C08B37/00C07K1/14C07K1/16C07K1/30C07K1/34C07K1/36
CPCC07H15/18C07H1/08C11B1/04C11B1/06C08B37/0003C08B37/006C07K1/36C07K1/34C07K1/30C07K1/16C07K1/145
Inventor 李石平
Owner 天水雪陆鱼生物科技有限责任公司
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