Environment-friendly interior wall putty powder and preparation method thereof
An interior wall putty powder, an environmentally friendly technology, applied in the direction of filling slurry, etc., can solve the problems of insufficient strength and hardness, poor stability of interior wall putty powder, etc.
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[0024] As a preferred embodiment, the average diameter of the boron nanofibers is 100-300 nm, and the aspect ratio is (10-16):1.
[0025] As a preferred embodiment, the coupling agent is at least one of silane coupling agent KH550, silane coupling agent KH560, and silane coupling agent KH570.
[0026] As a preferred embodiment, the preparation method of the co-modified octatetramethylcyclotetrasilazane of the polyether amide group comprises the following steps:
[0027] Step D1: Add single-ended epoxy polyether, octatetramethylcyclotetrasilazane, and basic catalyst into dimethyl sulfoxide, stir and react at 60-70°C for 4-6 hours, and then remove by rotary evaporation Dimethyl sulfoxide, dissolve the product with ether, filter to get the filtrate, and remove the ether by rotary evaporation to obtain polyether modified octatetramethylcyclotetrasilazane;
[0028] Step D2: Add the polyether-modified octatetramethylcyclotetrasilazane and chloroacetamide-N-methanol prepared in step...
Embodiment 1
[0047] An environment-friendly interior wall putty powder is characterized in that it is prepared from the following components in parts by weight: 4 parts of rosin polyether sulfonate, 3 parts of halloysite nanotubes, and 10 parts of white cement , 20 parts of inorganic filler, 5 parts of polyether-amide co-modified octatetramethylcyclotetrasilazane, 1 part of hydroxypropyl-β-cyclodextrin, 0.8 part of coupling agent, and 2 parts of nano-boron fiber.
[0048] The average diameter of the boron nanofiber is 100nm, and the aspect ratio is 10:1; the coupling agent is a silane coupling agent KH550.
[0049] The preparation method of described polyether-based amide co-modified octatetramethylcyclotetrasilazane comprises the steps of:
[0050] Step D1: Add single-ended epoxy polyether, octatetramethylcyclotetrasilazane, and basic catalyst into dimethyl sulfoxide, stir and react at 60°C for 4 hours, and then remove dimethyl sulfoxide by rotary evaporation , dissolve the product with ...
Embodiment 2
[0057] An environment-friendly interior wall putty powder is characterized in that it is prepared from the following components by weight: 4.5 parts of rosin polyether sulfonate, 3.5 parts of halloysite nanotubes, and 12 parts of white cement , 23 parts of inorganic fillers, 6 parts of polyether-amide co-modified octatetramethylcyclotetrasilazane, 1.2 parts of hydroxypropyl-β-cyclodextrin, 0.9 parts of coupling agent, and 2.5 parts of boron nanofibers.
[0058] The average diameter of the boron nanofiber is 150nm, and the aspect ratio is 12:1; the coupling agent is a silane coupling agent KH560.
[0059] The preparation method of described polyether-based amide co-modified octatetramethylcyclotetrasilazane comprises the steps of:
[0060] Step D1: Add single-ended epoxy polyether, octatetramethylcyclotetrasilazane, and basic catalyst to dimethyl sulfoxide, stir and react at 63°C for 4.5 hours, and then remove dimethyl sulfoxide by rotary evaporation , dissolve the product wit...
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