Carbon nitride-hydrotalcite heterogeneous material as well as preparation method and application thereof
A technology of heterogeneous material and hydrotalcite, applied in the field of photocatalytic materials, can solve problems such as low efficiency, and achieve the effects of simple synthesis method, easy operation of synthesis method, and good performance of decomposing water and hydrogen evolution
- Summary
- Abstract
- Description
- Claims
- Application Information
AI Technical Summary
Problems solved by technology
Method used
Image
Examples
Embodiment 1
[0032] A method for preparing a carbon nitride-hydrotalcite heterostructure for photocatalytic hydrogen production by hydrothermal method in this embodiment is specifically carried out according to the following steps:
[0033] 1) While stirring at 80°C, add 1 g of melamine into 70 times the volume of distilled water, stir for 60 min, then add 1.2 g of solid phosphorous acid, and continue stirring for 60 min;
[0034] 2) Transfer the solution obtained in step 1) to a reaction kettle, and heat it in an oven at a heating temperature of 180°C and a holding time of 10 hours;
[0035] 3) centrifuging the product obtained in step 2), the rotating speed is 4000r / min, and the centrifugation time is 3min;
[0036] 4) Put the product obtained in step 3) into a drying oven to dry at a drying temperature of 60°C and a drying time of 10 hours to obtain a precursor;
[0037] 5) Add the precursor (0.1g) obtained in step 4) to 40mL distilled water, then add 0.4mmoL nickel nitrate and 0.2mmoL...
Embodiment 2
[0043] A method for preparing a carbon nitride-hydrotalcite heterostructure for photocatalytic hydrogen production by a hydrothermal method in this embodiment is specifically carried out according to the following steps:
[0044] 1) With stirring at 80°C, add 1 g of melamine into 80 times the volume of distilled water, stir for 60 min, then add 1.2 g of solid phosphorous acid, and continue stirring for 60 min;
[0045] 2) Transfer the solution obtained in step 1) to a reaction kettle, and heat it in an oven at a heating temperature of 180°C and a holding time of 10 hours;
[0046] 3) centrifuging the product obtained in step 2), the rotating speed is 4000r / min, and the centrifugation time is 3min;
[0047] 4) Put the product obtained in step 3) into a drying oven to dry at a drying temperature of 60°C and a drying time of 10 hours to obtain a precursor;
[0048] 5) Add the precursor (0.1g) obtained in step 4) to 40mL distilled water, then add 0.8mmoL nickel nitrate and 0.4mmo...
Embodiment 3
[0054] A method for preparing a carbon nitride-hydrotalcite heterostructure for photocatalytic hydrogen production by a hydrothermal method in this embodiment is specifically carried out according to the following steps:
[0055] 1) With stirring at 80°C, add 1 g of melamine into 80 times the volume of distilled water, stir for 60 min, then add 1.2 g of solid phosphorous acid, and continue stirring for 60 min;
[0056] 2) Transfer the solution obtained in step 1) to a reaction kettle, and heat it in an oven at a heating temperature of 180°C and a holding time of 10 hours;
[0057] 3) centrifuging the product obtained in step 2), the rotating speed is 4000r / min, and the centrifugation time is 3min;
[0058] 4) Put the product obtained in step 3) into a drying oven to dry at a drying temperature of 60°C and a drying time of 10 hours to obtain a precursor;
[0059] 5) Add the precursor (0.1g) obtained in step 4) to 40mL distilled water, then add 1mmoL nickel nitrate and 0.5mmoL ...
PUM
Login to View More Abstract
Description
Claims
Application Information
Login to View More