High-strength flame-retardant insulation board and preparation method thereof
A flame-retardant heat preservation and high-strength technology, which is applied in the field of high-strength flame-retardant heat insulation board and its preparation, can solve the problems of impact resistance of polystyrene, performance of graphite polystyrene board, threat to life and property safety, etc., to achieve Not easy to agglomerate, improve strength and impact resistance, increase compatibility
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Embodiment 1
[0036] Preparation of modified expanded graphite
[0037] 100kg of expanded graphite with a particle size of 300-500 mesh was dispersed in absolute ethanol by ultrasonic, 4kg of titanate was added, heated to 50°C and ultrasonically impregnated for 3h, the ultrasonic frequency was 60kHz. Take out the expanded graphite and dry it in an oven at 85° C. to obtain modified expanded graphite.
Embodiment 2
[0039] Preparation of Modified Silica Airgel Particles
[0040] By spraying, once every 5 minutes, 2.5kg of isobutyltriethoxysilane was added to 100kg of silica airgel particles with a particle size of 0.5-1mm, and mixed for 1 hour at room temperature to obtain modified silica Silica airgel particles.
Embodiment 3
[0042] (1) Put 82.5kg of polystyrene, 5kg of chlorinated polyethylene, 1.0kg of polycaprolactone and 0.25kg of calcium stearate into a two-roller mill for blending, the temperature of the rollers is 180°C, and the milling is carried out for 20 minutes , to obtain a blend.
[0043] (2) The blend is mixed with 10kg modified expanded graphite, 2.5kg microencapsulated red phosphorus, 2kg modified silica airgel, 1.0kg polycaprolactone and 0.25kg calcium stearate to obtain a mixture .
[0044] (3) Send the mixture into the twin-screw extruder. The temperature of the first zone of the twin-screw extruder is 230°C, the temperature of the second zone is 235°C, the temperature of the third zone is 237°C, the temperature of the fourth zone is 240°C, and the temperature of the fifth zone The temperature is 245°C, the rotation speed of the main engine is 500rpm; the pore size of the filter is 50μm. After being extruded, it is cooled by the strands and pelletized to obtain graphite polyst...
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