Composite phase change powder material for selective laser sintering as well as preparation method and application of composite phase change powder material

A composite phase change and powder material technology, which is applied in heat exchange materials, chemical instruments and methods, etc., can solve the problems of large thermal cycle loss, uneven particle size distribution, and low powder sphericity of thermal management components, and achieves a reduction in Van der Waals force, high latent heat, good fluidity

Pending Publication Date: 2021-12-24
HUNAN UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0005] Existing phase-change powder materials, such as paraffin / expanded graphite composite phase-change powder materials, have defects such as poor powder fluidity, low powder sphericity, and uneven particle size distribution in phase-change powder materials, so they are used as selective laser sintering. When preparing thermal management components from raw materials, there are still defects such as poor molding accuracy and difficult control, and large thermal cycle losses of thermal management components.

Method used

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  • Composite phase change powder material for selective laser sintering as well as preparation method and application of composite phase change powder material
  • Composite phase change powder material for selective laser sintering as well as preparation method and application of composite phase change powder material
  • Composite phase change powder material for selective laser sintering as well as preparation method and application of composite phase change powder material

Examples

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Embodiment 1

[0039] A composite phase change powder material for selective laser sintering, the composite phase change powder material includes the following raw material components in parts by mass:

[0040] 80 parts of paraffin,

[0041] 15 parts of expanded graphite,

[0042] Micropowder silica gel 5 parts.

[0043] In this embodiment, the particle size of the composite phase change powder material is 50 μm˜150 μm, and the sphericity is 0.85.

[0044] The calculation formula of sphericity is as follows:

[0045]

[0046] Among them, V p is the particle volume, S p is the particle surface area.

[0047] A method for preparing a composite phase-change powder material for selective laser sintering in the above-mentioned embodiment, comprising the following steps:

[0048] (1) According to the mass ratio of 80:15:5 (calculated as 100 parts), respectively weigh paraffin wax, expanded graphite, and micropowdered silica gel.

[0049] (2) Put the weighed solid paraffin (melting point ...

Embodiment 2

[0053] A composite phase change powder material for selective laser sintering, the composite phase change powder material includes the following raw material components in parts by mass:

[0054] 85 parts of paraffin,

[0055] 10 parts of expanded graphite,

[0056] Micropowder silica gel 5 parts.

[0057] In this embodiment, the particle size of the composite phase-change powder material is 50 μm˜150 μm, and the sphericity is 0.93.

[0058] A method for preparing a composite phase-change powder material for selective laser sintering in the above-mentioned embodiment, comprising the following steps:

[0059] (1) According to the mass ratio of 85:10:5 (calculated as 100 parts), respectively weigh paraffin wax, expanded graphite, and micropowdered silica gel.

[0060] (2) Put the weighed solid paraffin (melting point is 56°C) into a planetary ball mill, pour -196°C liquid nitrogen into the ball mill tank to submerge the paraffin, and after the paraffin hardens, add manganese ...

Embodiment 3

[0064] A method for preparing a composite phase-change powder material for selective laser sintering is basically the same as in Example 2, the only difference being that in Example 3, the composite phase-change powder material includes the following raw material components in parts by mass:

[0065] 70 parts of paraffin,

[0066] 20 parts of expanded graphite,

[0067] Micronized silica gel 10 parts.

[0068] The particle size of the composite phase-change powder material prepared in Example 3 is 50 μm-150 μm, and the sphericity is 0.93.

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Abstract

The invention discloses a composite phase change powder material for selective laser sintering as well as a preparation method and application of the composite phase change powder material. The composite phase change powder material comprises the following raw material components in parts by mass: 70-89 parts of paraffin, 10-20 parts of expanded graphite and 1-10 parts of superfine silica powder. The preparation method comprises the following steps of: preparing the paraffin powder and the expanded graphite powder, mixing the paraffin powder and the expanded graphite powder with the superfine silica powder, cooling to-40 DEG C, grinding and sieving to obtain the composite phase change powder material. The composite phase change powder material has the advantages of high latent heat, high thermal conductivity, good fluidity and the like, can be used for selective laser sintering molding, can be widely used for production and manufacturing of thermal management parts, and has very high use value and application prospects. The preparation method of the composite phase change powder material has the advantages of being simple in process, convenient to operate, low in cost and the like, is suitable for industrial production and is beneficial to large-scale application.

Description

technical field [0001] The invention belongs to the technical field of preparation of laser sintering powder materials, and relates to a composite phase-change powder material for selective laser sintering, a preparation method and application thereof. Background technique [0002] Phase change materials refer to substances that change the state of matter and provide latent heat under the condition of constant temperature. The process of changing physical properties is called a phase change process, and the phase change material will absorb or release a large amount of latent heat at this time. As an important latent heat material, phase change materials have broad application prospects in the fields of heat storage and heat management. The advantages of high density, easy control of the process, approximately isothermal heat storage and release process, wide controllable temperature range, and stable chemical properties have become key materials in the field of thermal ene...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C09K5/06
CPCC09K5/063
Inventor 韩晓筱梁邦朝秦光照周丹陈锋
Owner HUNAN UNIV
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