Pellicle, exposure original plate with pellicle, method for producing semiconductor device, method for producing liquid crystal display panel, method for recycling exposure original plates, and method for reducing release residue
A technology of protective film and protective film, which is applied in semiconductor/solid-state device manufacturing, photolithography process exposure device, pressure-sensitive film/sheet, etc. It can solve the problems of difficult-to-expose original plate cleaning, etc., to ease cleaning conditions, improve production efficiency, damage reduction effect
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Embodiment 1
[0139] After precise cleaning of the pellicle frame made of aluminum alloy (outline dimensions: 149mm×115mm×3mm, wall thickness 2mm, flatness on the end surface side coated with adhesive for mask attachment: 15μm), on the end surface on the 15μm side, Apply an acrylic adhesive (product name: SK-Dyne SN-70A) manufactured by Soken Chemical Co., Ltd. over the entire circumferential direction of the end face and at the same width as the pellicle frame. , containing 95% by mass of the monomer component is an acrylic polymer containing an oxirane group-containing (meth)acrylate as a base material, and contains 2 % by mass (solid content) of polyvinyl ether compound), and left to stand at room temperature for 60 minutes. Thereafter, a spacer was placed on an aluminum plate having a flatness of 5 μm, and the pellicle frame coated with the adhesive was placed with the adhesive facing downward. As a result, the adhesive is processed flat in contact with the flat spacer.
[0140] Next,...
Embodiment 2
[0149] An acrylic adhesive manufactured by Soken Chemical Co., Ltd. (product name: SN-25B, 40% by mass of the monomeric component is an (meth)acrylic acid containing an oxirane group was used for the mask attachment adhesive. ester acrylic polymer as the base material), except that, the pellicle film completed in the same procedure as in Example 1 was attached to the same 6025 mask substrate as in Example 1.
[0150] In the same manner as in Example 1, after leaving the mask blank with the pellicle attached at room temperature for 24 hours, 193 nm ArF Laser at 10J / cm 2 UV rays are irradiated.
[0151] After being left at room temperature for 1 hour after ultraviolet irradiation, the pellicle was slowly peeled upward from the mask substrate at a speed of 0.1 mm / sec.
[0152] Visual observation of the mask blank after peeling revealed slightly thin streaks in the contour portion where the pellicle was attached. When the mass of the substrate after peeling was measured and com...
Embodiment 3
[0154] An acrylic adhesive manufactured by Soken Chemical Co., Ltd. (product name: SN-24C, containing 90% by mass of the monomer component is an (meth)acrylic acid containing an oxirane group was used as the adhesive for the mask. ester acrylic polymer as the base material), except that, the pellicle film completed in the same procedure as in Example 1 was attached to the same 6025 mask substrate as in Example 1.
[0155] In the same manner as in Example 1, after leaving the mask blank with the pellicle attached at room temperature for 24 hours, 193 nm ArF Laser at 10J / cm 2 UV rays are irradiated.
[0156] After being left at room temperature for 1 hour after ultraviolet irradiation, the pellicle was slowly peeled upward from the mask substrate at a rate of 0.1 mm / sec.
[0157] Visual observation of the mask blank after peeling revealed slightly thin streaks in the contour portion where the pellicle was attached. The mass of the substrate after peeling was measured, and com...
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Abstract
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