Animal cell culture microcarrier and preparation method thereof
A cell culture, microcarrier technology, applied in animal cells, vertebrate cells, biochemical equipment and methods, etc., can solve problems, safety of exogenous viruses in biological products, etc., achieve improved use efficiency, good water solubility and surface-active, easy-to-operate effects
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Embodiment 1
[0176] Preparation of microcarriers containing 2,3-epoxypropyltrimethylammonium chloride (GTA) and arginine (polyarginine) ligands.
[0177] (1) GTA cross-linked with dextran microspheres or dextran flakes
[0178] Take 100g of dextran and add it to a round bottom flask, add 1kg of pure water, stir well to make it swell, add 110g of Na 2 SO 4 , after stirring at 30°C for 1 hour, add 15ml of 1M sodium hydroxide solution into the round bottom flask, stir to dissolve, then raise the temperature to 55°C, add 50g of GTA to react for 8 hours. The product was washed three times with absolute ethanol, washed once with purified water, and filtered with suction to obtain a dextran-GTA gel.
[0179] (2) Allyl glyceryl ether activated dextran microspheres or flakes
[0180] Take 100 g of the dextran-GTA prepared in step (1) and put it into a round bottom flask, add 1 kg of pure water, add 70 g of sodium hydroxide, stir to dissolve, add allyl glyceryl ether, and react at 55 ° C for 12 h...
Embodiment 2
[0186] Preparation of microcarriers containing GTA and lysine (polylysine) ligands.
[0187] The operation steps are the same as in Example 1, and the arginine (polyarginine) in step 4) is replaced with lysine (polylysine).
Embodiment 3
[0189] Preparation of microcarriers containing arginine (polyarginine) ligands.
[0190] (1) Allyl glyceryl ether activated dextran microspheres or flakes
[0191] Take 100g of dextran and put it into a round bottom flask, add 1kg of purified water, stir well to make it swell, add 110g of Na 2 SO 4 , Add 70g of sodium hydroxide into the round bottom flask, stir to dissolve, add allyl glyceryl ether, and react at 55°C for 12 hours. After 12 hours, the activated gel was washed successively with 10 times the volume of purified water, ethanol and purified water.
[0192] (2) Brominated Allyl Glyceryl Ether
[0193] Take 1 L of the activated gel prepared in step (2) and put it into a round bottom flask, and add 250 mL of purified water and 30 g of anhydrous sodium acetate into the round bottom flask. After stirring well, add bromine water into the round bottom flask until the liquid in the bottle turns yellow. After bromination for 10 minutes, sodium formate was added to termi...
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