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Preparation method of flame-retardant shaving board based on double-layer coated ammonium polyphosphate microcapsule modification

A technology of double-layer coating of ammonium polyphosphate, which is applied in the field of preparation of flame-retardant particleboard based on double-layer coating of ammonium polyphosphate microcapsules, can solve the problems of poor flame-retardant effect and poor mechanical properties, and achieve improved mechanical properties. performance, good flame retardant effect, good flame retardant durability effect

Active Publication Date: 2022-04-12
TREEZO NEW MATERIAL TECH GRP CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0006] The invention provides a method for preparing flame-retardant particleboard based on the modification of double-layer coated ammonium polyphosphate microcapsules, which overcomes the above-mentioned deficiencies in the prior art, and can effectively solve the problem of poor flame-retardant effect and poor mechanical properties of the existing flame-retardant particleboard. poor performance problem

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0030] Example 1: The preparation method of the flame-retardant particle plate-based flame-retardant particle plate based on the double coated polyphosphate microcapsules, including the following steps:

[0031] S1: Aluminum hydroxide coated polyphosphate modification: adding polyphosphate to anhydrous ethanol and thoroughly stirring to form a suspension, adding a aluminum chloride solution and thoroughly stirring, adding an ammonia solution to the reaction, after completion, filtration, Wash, dry, to give ammonium ammonium alumina coated;

[0032] S2: Dopamine Double Coating Modification: Add Dopamlamine to deionized water to prepare a dopamine solution; then add the alumina prepared in step S1, ammonium hydroxide, stirred at room temperature, filtrate, wash, dried, dried. Get quadratic polyphosphate microcapsules;

[0033] S3: Preparation of a metal ionic salt solution: dissolve the metal salt in ion water to obtain a metal ionic salt solution, and the metal ion is selected from...

Embodiment 2

[0044] Example 2: The preparation method of the flame-retardant particle plate-based flame-retardant particleboard-based microcapsule modified double-layer coated polyphosphate, including the following steps:

[0045] S1: Aluminum hydroxide coated polyphosphate modification: adding polyphosphate to anhydrous ethanol and thoroughly stirring to form a suspension, adding a aluminum chloride solution and thoroughly stirring, adding an ammonia solution to the reaction, after completion, filtration, Wash, dry, to give ammonium ammonium alumina coated;

[0046] S2: Dopamine Double Coating Modification: Add Dopamlamine to deionized water to prepare a dopamine solution; then add the alumina prepared in step S1, ammonium hydroxide, stirred at room temperature, filtrate, wash, dried, dried. Get quadratic polyphosphate microcapsules;

[0047] S3: Preparation of a metal ionic salt solution: dissolve the metal salt in ion water to obtain a metal ionic salt solution, and the metal ion is selecte...

Embodiment 3

[0058] Example 3: This method of flame retardant particleboard preparation based on double-layer coated polyphosphate microcapsules, including the following steps:

[0059] S1: Aluminum hydroxide coated polyphosphate modification: adding polyphosphate to anhydrous ethanol and thoroughly stirring to form a suspension, adding a aluminum chloride solution and thoroughly stirring, adding an ammonia solution to the reaction, after completion, filtration, Wash, dry, to give ammonium ammonium alumina coated;

[0060] S2: Dopamine Double Coating Modification: Add Dopamlamine to deionized water to prepare a dopamine solution; then add the alumina prepared in step S1, ammonium hydroxide, stirred at room temperature, filtrate, wash, dried, dried. Get quadratic polyphosphate microcapsules;

[0061] S3: Preparation of a metal ionic salt solution: dissolve the metal salt in ion water to obtain a metal ionic salt solution, and the metal ion is selected from the group consisting of iron ions, cal...

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Abstract

The invention relates to the technical field of flame-retardant shaving board preparation, in particular to a flame-retardant shaving board preparation method based on double-layer coated ammonium polyphosphate microcapsule modification, which comprises the following steps: S1, aluminum hydroxide coated ammonium polyphosphate modification: ammonium polyphosphate is added into absolute ethyl alcohol and fully stirred to form a suspension, an aluminum chloride solution is added and fully stirred, and filtration is performed to obtain an aluminum hydroxide coated ammonium polyphosphate suspension; washing and drying to obtain aluminum hydroxide coated ammonium polyphosphate; s2, dopamine secondary coating modification: dopamine is added into deionized water, and a dopamine solution is prepared; then adding the aluminum hydroxide coated ammonium polyphosphate prepared in the step S1; s3, preparing a metal ion salt solution; s4, wood shaving modification; and S5, wood shaving sizing and paving. The preparation method is simple, easy to implement and capable of quickly adapting to the production process and technology of existing shaving boards, secondary processing equipment is avoided, cost is saved, and the prepared shaving boards have excellent mechanical property and flame retardant property.

Description

Technical field [0001] The present invention relates to the preparation of flame retardant particle plates, and is a method for preparing a flame-retardant particleboard based on double coated polyphosphate microcapsule modification. Background technique [0002] Particleboard is a kind of man-made panel, mainly based on wood or non-wood plant fiber feedstock, which is thermal and pressure to heat and pressure, and has a large, structure. Uniform, good processing performance, extensive source, low cost, etc., has been widely used in furniture, floor substrates, cabinets, custom wardrobes, building wall panels. However, since the particleboard is mainly composed of wood material, poor fire resistance is poor, it is easy to burn, and the fire is prone to fire, which limits the application range of particleboard. Therefore, the particleboard is flame retardant and imparted to its flame retardant properties. [0003] The ammonium polyphosphate (APP) is widely used, the price is low, ...

Claims

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Application Information

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IPC IPC(8): C04B26/12C04B111/28
Inventor 严玉涛陆铜华毕海明黄活阳魏任重周明吉郝玉东沈周
Owner TREEZO NEW MATERIAL TECH GRP CO LTD
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