Method for pretreating ardealite, ardealite crude product and recycled product
A phosphogypsum and pretreatment technology, applied in chemical instruments and methods, inorganic chemistry, calcium/strontium/barium sulfate, etc., can solve the problems of high energy consumption, high cost, unfriendly environment, etc., and achieve low energy consumption, The effect of low cost and low labor cost
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Embodiment 1
[0055] Place 1 ton of phosphogypsum in the drying room, continuously heat the phosphogypsum, and monitor the temperature, humidity and vapor pressure in the environment to perform the following process:
[0056] (1) Initial stage: In a closed environment, during the process of gradually rising temperature, the water in phosphogypsum enters the air, the ambient humidity increases, and the vapor pressure increases; the vapor pressure gradually reaches saturation, and the temperature of the system is 71°C. Humidity is 89%, reach the first condition, after maintaining for 5 minutes, proceed to the next step;
[0057] (2) The second dynamic environment stage: the airtight environment is released, the steam is discharged through the pipeline and condensed and collected, the steam pressure in the drying chamber drops, and the humidity drops; when the temperature is 90°C and the humidity reaches 71%, it is determined that the second condition is met ;Proceed to the next step;
[0058...
Embodiment 2
[0063] Place 1 ton of phosphogypsum in the drying room, continuously heat the phosphogypsum, and monitor the temperature, humidity and vapor pressure in the drying room at the same time, and perform the following process:
[0064] (1) Initial stage: In a closed environment, in the process of gradually rising temperature, the water in phosphogypsum enters the air, the ambient humidity increases, and the vapor pressure increases; the vapor pressure gradually reaches saturation, and the temperature of the system is 68°C. Humidity is 92%, reach the first condition, after maintaining for 7 minutes, proceed to the next step;
[0065] (2) The second dynamic environment stage: the airtight environment is released, the steam is discharged through the pipeline and condensed and collected, the steam pressure in the drying chamber drops, and the humidity drops; when the temperature is 88°C and the humidity reaches 72%, it is determined that the second condition is met ;Proceed to the next...
Embodiment 3
[0071] According to the method of Example 1, the difference is that in the first dynamic environment stage, instead of maintaining a period of time under the saturated vapor pressure environment, it will be exposed to a closed environment once the saturated vapor pressure is reached.
[0072] Other operations were the same as in Example 1, and after about 1h5min, the crude phosphogypsum and condensed water were finally obtained.
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