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Ferrosilicon nitride mullite silicon carbide brick for silicomanganese alloy ladle and preparation method of ferrosilicon nitride mullite silicon carbide brick

A mullite silicon carbide brick and ferrosilicon nitride technology, which is applied in metal processing equipment, manufacturing tools, casting equipment, etc., can solve the problems of slag erosion resistance, melt erosion resistance and thermal shock resistance. , Restricting the efficient and stable production of silicon-manganese alloys, frequent maintenance of alloy packages, etc., to achieve excellent resistance to slag erosion, ensure the quality of preparation, and improve the service life

Pending Publication Date: 2022-04-22
SHANDONG REFRACTORIES GROUP
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] The traditional silicon-manganese alloy-packed refractory bricks for smelting silicon-manganese alloys generally use high-alumina bricks, high-alumina silicon carbide bricks, etc., and their resistance to slag erosion, melt erosion and thermal shock resistance are all there Insufficient, so the service life is not high, the average package age is low, and the alloy package is frequently repaired, which restricts the efficient and stable production of silicon-manganese alloys

Method used

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  • Ferrosilicon nitride mullite silicon carbide brick for silicomanganese alloy ladle and preparation method of ferrosilicon nitride mullite silicon carbide brick
  • Ferrosilicon nitride mullite silicon carbide brick for silicomanganese alloy ladle and preparation method of ferrosilicon nitride mullite silicon carbide brick
  • Ferrosilicon nitride mullite silicon carbide brick for silicomanganese alloy ladle and preparation method of ferrosilicon nitride mullite silicon carbide brick

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0035] A Si-Mn alloy-coated ferrosilicon nitride-mullite silicon carbide brick, comprising the following raw materials in mass percentage:

[0036]

[0037] The moisture mass content of silicon carbide and ferrosilicon nitride fine powder in the raw materials is all ≤0.3%, and the moisture mass content of other raw materials is all ≤0.5%.

[0038] The preparation method of the silicon-manganese alloy-coated ferrosilicon nitride-mullite silicon carbide brick comprises the following steps:

[0039] Add the prepared granules into the mixer and stir for 2 minutes, then add the weighed binding solution, mix for 3 minutes, then add the weighed fine powder, mix for 5 minutes, and discharge after mixing evenly. Mix and stir for no less than 12 minutes; use a double-screw program-controlled 630T press for molding, use the first blow at a speed of 180 rpm, and then exhaust once, and then increase the speed at each gear to 50 rpm, and press to five gears; After drying, the temperatur...

Embodiment 2

[0041] A Si-Mn alloy-coated ferrosilicon nitride-mullite silicon carbide brick, comprising the following raw materials in mass percentage:

[0042]

[0043] The moisture mass content of silicon carbide and ferrosilicon nitride in the raw materials are all ≤0.3%, and the moisture content of other raw materials are all ≤0.5%.

[0044] The preparation method of the silicon-manganese alloy-coated ferrosilicon nitride-mullite silicon carbide brick comprises the following steps:

[0045] Put the prepared granules into the mixer and stir for 2 minutes, then add the weighed binding solution, mix for 5 minutes, then add the weighed fine powder, mix for 8 minutes, and discharge after mixing evenly. Mix and stir for no less than 12 minutes; use a double-screw program-controlled 630T press for molding, use the first blow at a speed of 180 rpm, and then exhaust once, and then increase the speed at each gear to 50 rpm, and press to five gears; After drying, the temperature is raised at ...

Embodiment 3

[0047] A Si-Mn alloy-coated ferrosilicon nitride-mullite silicon carbide brick, comprising the following raw materials in mass percentage:

[0048]

[0049]

[0050] The moisture mass content of silicon carbide and ferrosilicon nitride in the raw materials are all ≤0.3%, and the moisture content of other raw materials are all ≤0.5%.

[0051] The preparation method of the silicon-manganese alloy-coated ferrosilicon nitride-mullite silicon carbide brick comprises the following steps:

[0052] Add the prepared granules into the mixer and stir for 2 minutes, then add the weighed binding solution, mix for 4 minutes, then add the weighed fine powder, mix for 6 minutes, and discharge after mixing evenly. Mix and stir for no less than 12 minutes; use a double-screw program-controlled 630T press for molding, use the first blow at a speed of 180 rpm, and then exhaust once, and then increase the speed at each gear to 50 rpm, and press to five gears; After drying, the temperature i...

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Abstract

The invention relates to a ferro-silicon nitride mullite silicon carbide brick for a silicon-manganese alloy ladle and a preparation method of the ferro-silicon nitride mullite silicon carbide brick, and belongs to the technical field of silicon-manganese alloy ladle linings. The silicon iron nitride mullite silicon carbide brick is prepared from the following raw materials in percentage by mass: 15 to 20 percent of 5 to 3 mm alumina, 15 to 25 percent of 1 to 0 mm alumina, 19 to 24 percent of 0.074 mm alumina fine powder, 18 to 26 percent of 3 to 1 mm mullite, 1 to 5 percent of 1 to 0 mm silicon carbide, 2 to 8 percent of 0.074 mm silicon carbide fine powder, 2 to 6 percent of 0.074 mm alumina powder, 1 to 4 percent of 0.074 mm silicon iron nitride, 4 to 9 percent of 0.074 mm Guangxi white mud and 1 to 2 percent of 0.074 mm metal silicon powder. The product provided by the invention has excellent slag corrosion resistance, melt scouring resistance and thermal shock resistance, and the service life is obviously prolonged; meanwhile, the invention provides a preparation method beneficial to industrial production.

Description

technical field [0001] The invention relates to a ferrosilicon nitride mullite silicon carbide brick coated with a silicon-manganese alloy and a preparation method thereof, belonging to the technical field of silicon-manganese alloy lining. Background technique [0002] At present, silicon-manganese alloy is an alloy composed of manganese, silicon, iron and a small amount of carbon and other elements. It is a ferroalloy with wide application and large output. Manganese-silicon alloy is a compound deoxidizer commonly used in steelmaking, and it is also a reducing agent for the production of medium and low carbon ferromanganese and the production of metal manganese by electrosilicothermal method. The market demand is huge. [0003] The traditional silicon-manganese alloy-packed refractory bricks for smelting silicon-manganese alloys generally use high-alumina bricks, high-alumina silicon carbide bricks, etc., and their resistance to slag erosion, melt erosion and thermal shock...

Claims

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Application Information

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IPC IPC(8): C04B35/103C04B35/622C04B35/626C04B35/64B22D41/02
CPCC04B35/103C04B35/622C04B35/62605C04B35/64B22D41/02C04B2235/3826C04B2235/3463C04B2235/428C04B2235/3873C04B2235/3852C04B2235/349C04B2235/5427C04B2235/5436C04B2235/656C04B2235/6567C04B2235/9607C04B2235/9669C04B2235/9676
Inventor 李宗宝任建秀汪继炉
Owner SHANDONG REFRACTORIES GROUP
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