Preparation method of epoxy resin-based heat-conducting, heat-resisting and electric-conducting adhesive film
A technology of epoxy resin and conductive adhesive film, applied in epoxy resin adhesive, conductive adhesive, film/sheet adhesive and other directions, can solve the problems of cracking and deformation, chip side climbing glue, chip tilting and other problems , to achieve high-efficiency anti-aging effect and good manufacturability
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Embodiment 1
[0038] This embodiment is an epoxy resin-based heat-conducting heat-resistant conductive adhesive film, including the following components by weight:
[0039] 12 parts of epoxy resin, 2 parts of diluent, 5 parts of curing agent, 5 parts of coupling agent, 3 parts of conductive accelerator, 5 parts of anti-aging agent, 120 parts of silver powder;
[0040] The epoxy resin-based heat-conducting heat-resistant conductive adhesive film is prepared by the following steps:
[0041] S1: Mix the epoxy resin and the conductive accelerator evenly, and grind them thoroughly;
[0042] S2: Add silver powder, mix evenly, vacuumize, then add diluent, coupling agent and anti-aging agent and mix evenly;
[0043] S3: adding a curing agent and mixing evenly, and vacuumizing to obtain the epoxy resin-based heat-conducting heat-resistant conductive adhesive film;
[0044] Anti-aging agent is prepared by the following steps:
[0045] S11: Under the condition of ice bath, add 46mL of concentrated ...
Embodiment 2
[0052] This embodiment is an epoxy resin-based heat-conducting heat-resistant conductive adhesive film, including the following components by weight:
[0053] 10 parts of epoxy resin, 1 part of diluent, 1 part of curing agent, 5 parts of coupling agent, 3 parts of conductive accelerator, 5 parts of anti-aging agent, 100 parts of silver powder;
[0054] The epoxy resin-based heat-conducting heat-resistant conductive adhesive film is prepared by the following steps:
[0055] S1: Mix the epoxy resin and the conductive accelerator evenly, and grind them thoroughly;
[0056] S2: Add silver powder, mix evenly, vacuumize, then add diluent, coupling agent and anti-aging agent and mix evenly;
[0057] S3: adding a curing agent and mixing evenly, and vacuumizing to obtain the epoxy resin-based heat-conducting heat-resistant conductive adhesive film;
[0058] Anti-aging agent is prepared by the following steps:
[0059] S11: Under the condition of ice bath, add 46mL of concentrated H ...
Embodiment 3
[0066] This embodiment is an epoxy resin-based heat-conducting heat-resistant conductive adhesive film, including the following components by weight:
[0067] 10 parts of epoxy resin, 2 parts of diluent, 5 parts of curing agent, 5 parts of coupling agent, 3 parts of conductive accelerator, 5 parts of anti-aging agent, 120 parts of silver powder;
[0068] The epoxy resin-based heat-conducting heat-resistant conductive adhesive film is prepared by the following steps:
[0069] S1: Mix the epoxy resin and the conductive accelerator evenly, and grind them thoroughly;
[0070] S2: Add silver powder, mix evenly, vacuumize, then add diluent, coupling agent and anti-aging agent and mix evenly;
[0071] S3: adding a curing agent and mixing evenly, and vacuumizing to obtain the epoxy resin-based heat-conducting heat-resistant conductive adhesive film;
[0072] Anti-aging agent is prepared by the following steps:
[0073] S11: Under the condition of ice bath, add 46mL of concentrated ...
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