Method for treating coating waste liquid of lithium ion battery diaphragm
A lithium-ion battery and waste liquid treatment technology, applied in water/sewage treatment, chemical instruments and methods, multi-stage water/sewage treatment, etc., can solve problems such as inability to use directly, easily pollute the environment, and low concentration of waste water, and achieve Effects of extended service life, high concentration, and improved purity
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preparation example 1
[0049] Preparation method of nanosulfonated polystyrene microspheres, comprising the following steps:
[0050] (1) 12kg styrene monomer, 2kg of sodium lauryl sulfate, 3kg of sodium bicarbonate and 2kg of azo diisobutyronitrile were added to the water, heated to 65 °C, the reaction was 18h, and the solid product was washed and dried to obtain nano polystyrene microspheres;
[0051] (2) The nano polystyrene microspheres obtained in step (1) were added to the concentrated sulfuric acid, and the sulfonation reaction at 55 °C was 2h, and the reaction product was washed and dried to give the nano-sulfonated polystyrene microspheres.
preparation example 2
[0053] Preparation method of nanosulfonated polystyrene microspheres, comprising the following steps:
[0054](1) 12kg styrene monomer, 2kg sodium lauryl sulfate, 3kg sodium bicarbonate and 2kg azo diisobutyronitrile were added to water, heated to 75 °C, the reaction was 10h, and the solid product was washed and dried to give nano polystyrene microspheres;
[0055] (2) The nano polystyrene microspheres obtained in step (1) were added to the concentrated sulfuric acid, and the sulfonation reaction was 8h at 30 °C, and the reaction product was washed and dried to give the nano-sulfonated polystyrene microspheres.
preparation example 3
[0057] The difference from the preparation example 1 is that the emulsifier uses polyoxyethylene stearate.
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