Three-dimensional titanium fluoride-based organic self-assembly complex for in-situ growth of titanium oxide as well as preparation method and application of three-dimensional titanium fluoride-based organic self-assembly complex
A technology of three-dimensional titanium fluoride and titanium oxide, which is applied in organic compound/hydride/coordination complex catalysts, chemical instruments and methods, water treatment of special compounds, etc., can solve problems such as instability, achieve low cost, Good adsorption activity and enhanced photocatalytic activity
- Summary
- Abstract
- Description
- Claims
- Application Information
AI Technical Summary
Problems solved by technology
Method used
Image
Examples
Embodiment 1
[0023] In the present embodiment, the specific steps for preparing the synthesized three-dimensional titanium fluoride-based organic self-assembled complex of in-situ grown titanium oxide are as follows:
[0024] 1) Disperse 2492.0 mg of terephthalic acid uniformly in 5 mL of methanol and 45 mL of N,N-dimethylformamide (DMF), then add 1.3 mL of titanium tetraisopropoxide, and stir to make the solution uniform;
[0025] 2) Then the solution was transferred into a reaction kettle with 100 mL of polytetrafluoroethylene lining, heated in a forced air drying oven at 150 ° C for 15 h, cooled to room temperature, and centrifuged, and then washed with N,N-dimethylformamide and After washing with methanol three times, it was kept under vacuum at 60 °C for 24 h, and white powder was obtained by grinding, namely three-dimensional titanium-based organic self-assembled complexes;
[0026] 3) 60 mg of the obtained powder three-dimensional titanium-based organic self-assembled complex, 10 mg...
Embodiment 2
[0028] 1) Disperse 2492.0 mg of terephthalic acid uniformly in 5 mL of methanol and 45 mL of N,N-dimethylformamide (DMF), then add 1.3 mL of titanium tetraisopropoxide, and stir to make the solution uniform;
[0029] 2) Then the solution was transferred into a reaction kettle with 100 mL of polytetrafluoroethylene lining, heated in a forced air drying oven at 150 ° C for 15 h, cooled to room temperature, and centrifuged, and then washed with N,N-dimethylformamide and After washing with methanol three times, it was kept under vacuum at 60 °C for 24 h, and white powder was obtained by grinding, namely three-dimensional titanium-based organic self-assembled complexes;
[0030] 3) 60 mg of the obtained powder three-dimensional titanium-based organic self-assembly complex, 20 mg of sodium fluoride and 100 mg of tannic acid were added to 60 mL of ultrapure water, and the suspension was transferred to a reaction kettle with 100 mL of polytetrafluoroethylene lining, Heating in an oven...
Embodiment 3
[0032] 1) Disperse 2492.0 mg of terephthalic acid uniformly in 5 mL of methanol and 45 mL of N,N-dimethylformamide (DMF), then add 1.3 mL of titanium tetraisopropoxide, and stir to make the solution uniform;
[0033] 2) Then the solution was transferred into a reaction kettle with 100 mL of polytetrafluoroethylene lining, heated in a forced air drying oven at 150 ° C for 15 h, cooled to room temperature, and centrifuged, and then washed with N,N-dimethylformamide and After washing with methanol three times, it was kept under vacuum at 60 °C for 24 h, and white powder was obtained by grinding, namely three-dimensional titanium-based organic self-assembled complexes;
[0034] 3) 60 mg of the obtained powder three-dimensional titanium-based organic self-assembled complex, 50 mg of sodium fluoride and 120 mg of tannic acid were added to 60 mL of ultrapure water, and the suspension was transferred to a reaction kettle with 100 mL of polytetrafluoroethylene lining, Heating in an ove...
PUM
Login to View More Abstract
Description
Claims
Application Information
Login to View More - R&D
- Intellectual Property
- Life Sciences
- Materials
- Tech Scout
- Unparalleled Data Quality
- Higher Quality Content
- 60% Fewer Hallucinations
Browse by: Latest US Patents, China's latest patents, Technical Efficacy Thesaurus, Application Domain, Technology Topic, Popular Technical Reports.
© 2025 PatSnap. All rights reserved.Legal|Privacy policy|Modern Slavery Act Transparency Statement|Sitemap|About US| Contact US: help@patsnap.com