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Preparation method of powder injection molding beta-type titanium alloy feed

A powder injection molding, titanium alloy technology, applied in metal processing equipment, transportation and packaging, etc., can solve the problems of narrow application fields, restricting the industrialization process of titanium alloy injection molding, and short application time of titanium alloy injection molding technology, and achieve The effect of expanding the scope of application

Active Publication Date: 2022-07-12
深圳市泛海统联精密制造股份有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] However, the application time of titanium alloy injection molding technology is still relatively short, and the application field is relatively narrow. Many powders required for titanium alloy injection molding cannot be directly produced, which restricts the industrialization process of titanium alloy injection molding.

Method used

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  • Preparation method of powder injection molding beta-type titanium alloy feed
  • Preparation method of powder injection molding beta-type titanium alloy feed
  • Preparation method of powder injection molding beta-type titanium alloy feed

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0027] Weigh 12000 g of Ti64 titanium alloy (Ti6Al4V) powder, D50=12-14 microns; 2048 g of metal vanadium powder, 500 mesh; 16 g of stearic acid, powder particle size of 0.2-0.3 mm.

[0028] The above three kinds of powders were put into the mixing barrel and mixed thoroughly for 12 hours to obtain Ti518 powder.

[0029] Take 4250g of mixed Ti518 powder into the mixing chamber of the mixer, heat at 175°C for 10 minutes, then add 600g of copolymerized polyoxymethylene (9520), 125g of lubricant (PW) and 25g of BASF (B215) in turn, and continue After mixing for 30 minutes, during the mixing process, argon gas was introduced into the mixing chamber for protection under positive pressure, and the argon gas pressure was 1.2Mpa. After the mixing is completed, the pellets are diced and cooled to obtain β-type titanium alloy feedstock Ti518 (Ti5Al18V).

Embodiment 2

[0031] Take 4500g of Ti518 powder mixed in Example 1 and add it to the mixing chamber of the mixer, heat at 175°C for 10 minutes, then add 400g of copolymerized polyoxymethylene (9520), 95g of lubricant (PW) and BASF (B215) in turn. ) 5g, and continued to mix for 30 minutes. During the mixing process, argon was introduced into the mixing chamber for protection under positive pressure, and the argon pressure was 1.2Mpa. After the mixing is completed, the pellets are diced and cooled to obtain β-type titanium alloy feedstock Ti518 (Ti5Al18V).

Embodiment 3

[0033] Take 4435g of Ti518 powder mixed in Example 1 into the mixing chamber of the mixer, heat at 175 ° C for 10 minutes, then add 500g of copolymerized polyoxymethylene (9520), 50g of lubricant (PW) and BASF (B215 ) 15g, and continued to mix for 30 minutes. During the mixing process, argon was introduced into the mixing chamber for protection under positive pressure, and the argon pressure was 1.2Mpa. After the mixing is completed, the pellets are diced and cooled to obtain β-type titanium alloy feedstock Ti518 (Ti5Al18V).

[0034] The β-type titanium alloys prepared in Examples 1-3 were taken as feeding materials, and three groups of β-type titanium alloy tensile workpieces were obtained by injection molding respectively.

[0035] Place the β-type titanium alloy drawn workpiece on a high-purity zirconia ceramic plate, and then put it into a degreasing furnace for degreasing. Set degreasing temperature 100℃, nitrogen flow 5m 3 / h, the acid amount is 200ml / h, after the degr...

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Abstract

The invention discloses a preparation method of a powder injection molding beta-type titanium alloy feed. The preparation method comprises the following steps that Ti64 titanium alloy powder, vanadium powder and stearic acid are taken and mixed for 12 h, and Ti518 powder is obtained; ti518 powder is taken and heated for 10 minutes at the temperature of 175 DEG C, then polyformaldehyde, a lubricant and an antioxidant are sequentially added, mixing continues for 30 minutes, argon positive pressure protection is used in the mixing process, and the pressure is 1.2 Mpa; according to the method, a new titanium alloy mark is obtained by mixing the spheroidized titanium alloy powder and the metal vanadium powder, the method is the only method for obtaining the beta-type titanium alloy feed through injection molding at present, the technical blank of titanium alloy powder injection molding is filled, and the application range of titanium alloy powder injection molding is widened.

Description

technical field [0001] The invention relates to the technical field of metal powder injection molding, in particular to a preparation method for powder injection molding beta-type titanium alloy feed. Background technique [0002] Titanium alloy has the advantages of low density, good biocompatibility, excellent corrosion resistance, good wear resistance and high specific strength, and is one of the metal materials favored by consumer electronic products. At present, many products including bracelets, smart watches, hearing aids and other products have widely used titanium alloys to make shells and key components. However, titanium alloys have problems such as low thermal conductivity and obvious work hardening phenomenon. Conventional machining methods are difficult to process, low in efficiency and expensive in processing equipment. [0003] At present, domestic titanium and titanium alloys are classified into TA type, TB type and TC type according to traditional standard...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): B22F1/10B22F3/22C22C1/04C22C14/00
CPCB22F3/225C22C1/0458C22C14/00
Inventor 张新房侯春伟杨虎陈宏亮
Owner 深圳市泛海统联精密制造股份有限公司