Aerogel composite electrochromic glass and preparation method thereof
An electrochromic glass and aerogel technology, applied in climate change adaptation, instruments, optics, etc., can solve the problem of not being able to meet the energy-saving needs in winter and summer at the same time, and achieve the improvement of visible light transmittance in faded state and automatic color adjustment. , the effect of improving conductivity
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[0045] A preparation method of aerogel composite electrochromic glass, comprising the following steps:
[0046] Step 1: Prepare the first substrate 11: Select high-quality float glass and wash it with deionized water, then transfer it to a magnetron sputtering coating machine, and an RF plasma cleaning device is installed in the buffer chamber of the coating machine. After plasma cleaning, spray optical Absorber to prepare the first substrate 11;
[0047] Step 2. Preparation of bottom layer Bi 4 O 6 Layer: The first substrate 11 after the first step is sent to the coating area, the bismuth target is magnetron sputtered, the DC power supply is reactive sputtering, and Ar gas, O 2 As a sputtering gas, the gas flow rate is 100SCCM: 120SCCM, the film thickness is 20-40nm, and the bottom layer is obtained;
[0048] Step 3: Prepare the first anti-reflection dielectric film layer 12: The substrate completed in Step 2 is sent to the next coating area, and the DC power supply is rea...
Embodiment 1
[0073] During the preparation of the cathode discoloration layer in Example 1, WO 3 , MO 3 The powder doping ratio is 1:2; when the PVB cast film layer is prepared, the PVB resin is 600g, lithium salt 300g, 150g plasticizer, 15g ultraviolet absorber, 20g stabilizer, and the lithium salt is composed of carbonic acid. Lithium and lithium niobate are composed according to the weight ratio of 1:1, and the measured conductivity of the PVB cast film is 10. -5 S / cm;
Embodiment 2
[0074] In the preparation of the cathode discoloration layer in Example 2, WO 3 , MO 3 The powder doping ratio is 1.2:2; when the PVB cast film layer is prepared, the PVB resin is 500g, the lithium salt is 200g, the plasticizer is 150g, the ultraviolet light absorber is 15g, and the stabilizer is 20g. Lithium chlorate and lithium niobate are composed according to the weight ratio of 1:1, and the measured conductivity of PVB cast film is 10. -5 S / cm;
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