Low temperature sintered very high frequency laminated sheet type electrical inductance, sheet type magnetic beal material and its preparation method
A VHF laminated chip and VHF technology, which is applied in the material and preparation field of a VHF laminated chip inductor or chip magnetic bead, can solve the problem that the maximum use frequency is only 100MHz, etc. To achieve the effects of easy control of process parameters, wide application prospects and simple preparation methods
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Embodiment 1
[0033] Embodiment 1, adopts analytically pure Fe 2 o 3 、BaCO 3 , SrCO 3 , PbO, Co 3 o 4 , ZnO, CuO as initial raw materials, molar ratio Fe 2 o 3 : BaCO 3 : SrCO 3 :PbO:Co 3 o 4 : ZnO: CuO = 1: 0.2: 0.1: 0.09: 0.1: 0.24: 0.12 Weighed, ball milled and mixed with absolute ethanol for 24 hours, dried at 70-100°C, passed through a 200-mesh sieve, and tested at 1000°C and 1050°C , 1100 ℃ pre-burning, heat preservation for 6 hours, 4 hours, 2 hours, to obtain pure single-phase Y-type soft magnetic ferrite powder; the obtained Y-type ferrite powder and the raw material as Bi 2 o 3 +Al 2 o 3 +PbO+B 2 o 3 +SiO2 2 +CaF 2 The composite low-fired sintering aid mixed with equal amounts of LiF is mixed according to the weight ratio of 5%, 3%, and 1% with the weight of ferrite powder, ball milled for 24 hours, dried and sieved, granulated, and formed, respectively at 850 °C, 890 °C and 920 °C for 10 hours, 6 hours, and 0.5 hours for sintering and heat preservation, which ar...
Embodiment 2
[0035] Embodiment 2, adopt analytically pure Fe 2 o 3 、BaCO 3 , SrCO 3 , PbO, Co 3 o 4 , ZnO, CuO as initial raw materials, molar ratio Fe 2 o3 : BaCO 3 : SrCO 3 :PbO:Co 3 o 4 : ZnO: CuO = 1: 0.3: 0.05: 0.01: 0.13: 0.1: 0.22 Weighed, ball milled and mixed with absolute ethanol for 24 hours, dried, passed through a 200-mesh sieve, and tested at 900°C, 950°C, 1000°C, Pre-fire at 1050°C, keep warm for 6 hours, 4 hours, 3 hours, 2 hours to obtain pure single-phase Y-type soft ferrite powder. Gained ferrite powder and take raw material as Bi 2 o 3 +Al 2 o 3 +PbO+B 2 o 3 +SiO2 2 +CaF 2 Composite low-fired sintering aid mixed with equal amounts of +LiF, mixed according to the weight ratio of 5%, 4%, 2%, 1% to the weight of ferrite powder, ball milled for 24 hours, dried and sieved, granulated, and formed , were sintered at 850°C, 870°C, 900°C and 920°C for 10 hours, 6 hours, 4 hours, and 0.5 hours, respectively, and were recorded as samples 2-1, 2-2, 2-3, and 2-4. ...
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