Nano anti-wear agent, and preparing method and use thereof

A nano-anti-wear and carbon nano-tube technology, which is applied in the direction of additives, petroleum industry, lubricating compositions, etc., can solve the problems of no anti-wear and anti-friction characteristics, and promote wear, so as to achieve extended service life, good extreme pressure, and friction The effect of low coefficient

Inactive Publication Date: 2005-10-19
深圳市龙岗区华宇新材料研究中心
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Commonly used surface modifiers include dialkyl dithiophosphoric acid, alkyl phosphate, oleic acid, stearic acid, titanium ester acid coupling agent, organic silicon, nitrogen-containing organic compounds, etc. Mixing nanoparticles, if the dispersant is not properly selected, once it is added to the lubricating oil, it will not only have no anti-wear and anti-friction properties, but will promote wear

Method used

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  • Nano anti-wear agent, and preparing method and use thereof

Examples

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Comparison scheme
Effect test

example 1

[0017] Example 1. Nano antiwear agent

[0018] 1. Composition: The weight percentages of polyisobutylene and carbon nanotubes are 50-99 and 1-50 respectively.

[0019] 2. the method for preparing nanometer antiwear agent, its step comprises:

[0020] (1) Mix polyisobutylene and carbon nanotubes in proportion, and the weight percentages are 50-99 and 1-50 respectively (see attached table),

[0021] (2) Stir evenly, or put into a ball mill to mix well,

[0022] (3) Grind in a three-roll mill, or disperse with an ultrasonic machine for 25 to 35 minutes.

[0023] The following steps may also be included:

[0024] (4) heat insulation and heating to reconcile, this step can speed up the reconciliation. The heating temperature is generally controlled at 40-90°C for 10-20 minutes.

[0025] The prepared product is the concentrated solution of the nanometer antiwear agent.

example 2

[0026] Example 2. Nano lubricating oil

[0027] 1. Composition: The weight percentages of nano antiwear agent and carbon nanotube are 3 and 97 respectively.

[0028] 2. Preparation method: mix the two materials of nanometer anti-wear agent and lubricating oil in proportion, stir them evenly, or make them after heat insulation, heating, reconciliation and cooling.

[0029] The nanometer anti-wear agent of example 1 is selected for use, which is a concentrated solution.

example 3

[0030] Example 3. Engine automatic repair agent

[0031] 1. Composition: the weight percentages of nano antiwear agent and lubricating oil are 80 and 20 respectively.

[0032] 2. Preparation method: mix the two materials of nanometer anti-wear agent and lubricating oil in proportion, stir them evenly, or make them after heat insulation, heating, reconciliation and cooling.

[0033] The nanometer anti-wear agent of example 1 is selected for use, which is a concentrated solution.

[0034] 2. Schedule

[0035] Composition and proportioning (weight %) of nano antiwear agent

[0036]

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Abstract

The invention is a kind of nano antiwear additive and the manufacturing method and the application. The nano antiwear additive is made up of polyisobutylene and carbon nano pipe, the proportion of each ingredients are: 50-99, 1-50. the producing steps include: mixing the polyisobutylene, carbon nano pipe according to a proportion; stirring them or putting them into the globe mill; putting them into the triple-roller mill, or using supersonic wave machine to carry on decncentration for 25-35 minutes. It uses 3% nano antiwear additive and 97% lubricating oil to produce nano lubricating oil, uses 80% nano antiwear additive and 20% lubricating oil as automatic renovation agent, the producing method is: nano antiwear additive, lubricating oil are mixed together, and gets the product through heating, and cooling.

Description

technical field [0001] The invention relates to the field of chemical industry, in particular to a nanometer anti-wear agent and its preparation method and application. Background technique [0002] At present, research on the application of nanomaterials in various related fields has been carried out, but at the same time, they are faced with the problems of extremely small particle size, large specific surface area, high surface energy, and easy agglomeration between particles. Therefore, dispersion stability is still the key to the application of nanoparticles in tribology. For example, most of the wear particles of internal combustion engine lubricating oil are nanoparticles, because they cannot be well dispersed in the lubricating oil, and the particles formed after agglomeration not only cannot resist and reduce wear, but will promote wear. In addition, the nanoparticles without surface modification were directly added to the base oil, and after being forcibly dispers...

Claims

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Application Information

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IPC IPC(8): C10M143/06
Inventor 李幼清徐平
Owner 深圳市龙岗区华宇新材料研究中心
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