Process for producing organic compound using nitrite
A technology for organic compounds and nitroso compounds, which is applied in the preparation of organic compounds, organic chemical methods, and preparation of nitro compounds, and can solve problems such as low space-time yields and harsh reaction conditions
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Embodiment 1
[0118] Cyclopentane (1ml), tert-butyronitrile (1mmol), N-hydroxyphthalimide (0.2mmol) and acetic acid (1ml) were put into a flask and heated under an argon atmosphere (1atm=0.101 MPa) for 20 hours. Analysis of the resulting reaction mixture revealed formation of cyclopentanone oxime, nitrocyclopentane, cyclopentanone and cyclopentyl acetate in yields of 4%, 2%, 3% and less than 1%, respectively.
Embodiment 2
[0120] Cyclohexane (1ml), tert-butyronitrile (1mmol), N-hydroxyphthalimide (0.2mmol) and acetic acid (1ml) were put into the flask and heated under an argon atmosphere (1atm=0.101 MPa) for 20 hours. Analysis of the resulting reaction mixture revealed the formation of cyclohexanone oxime, nitrocyclohexane, cyclohexanone and cyclohexyl acetate in yields of 16%, 10%, 3% and 2%, respectively.
Embodiment 3
[0122] Cyclohexane (1ml), tert-butyronitrile (1mmol), 4-chloro-N-hydroxyphthalimide (0.2mmol) and acetic acid (1ml) were put into a flask and heated at 80°C under an argon atmosphere (1 atm = 0.101 MPa) and stirred for 20 hours. Analysis of the resulting reaction mixture revealed the formation of cyclohexanone oxime, nitrocyclohexane, cyclohexanone and cyclohexyl acetate in yields of 13%, 9%, 2% and 2%, respectively.
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