Method of synthesizing methyl carbamate

A technology for the synthesis of methyl carbamate and methanol, which is applied in the preparation of carbamic acid derivatives, chemical instruments and methods, and the preparation of organic compounds, and can solve problems such as low carbamate yield, poor selectivity, and harsh reaction conditions

CN1475481AInactive Publication Date: 2004-02-18PETROCHINA CO LTD +1
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Patent Information

Authority / Receiving Office
CN · China
Patent Type
Applications(China)
Current Assignee / Owner
Publication Date
2004-02-18
Estimated Expiration
Not applicable · inactive patent
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Abstract

A process for synthesizing methyl aminoformate includes the catalytic reaction between methanol, urea and catalyst at 120-200 deg.C, under 0.1-3 MPa for 0.5-20 hr and condensing and recovering ammonia gas. Its advantages are low cost and high selectivity to product.
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Description

[0001] Field:

[0002] The invention belongs to a method for synthesizing methyl carbamate. Background technique:

[0003] Methyl Carbomate (MC for short), also known as urethane, is an intermediate in organic synthesis, mainly used in the manufacture of herbicides, pesticides and plastic processing, and can also be used in the synthesis of sleeping pills, sedatives, and nux. Alkali, resorcinol antidotes, injections, cosolvents and coloring agents in the printing and dyeing industry can also be used as biochemical reagents for biochemical research. At the same time, methyl carbamate is the reaction raw material for the synthesis of dimethyl carbonate.

[0004] Early methyl carbamate was mainly produced by the reaction of amines and phosgene or chloroformate, which not only seriously polluted the environment but also had high production costs. In recent years, foreign countries have successively developed a new process for preparing methyl carbamate from the reaction of carbo...

Examples

Embodiment 1

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