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Nickel oxide nano electrochromism film and preparing method thereof

An electrochromic and nickel oxide technology, which is applied in the direction of chemical instruments and methods, luminescent materials, etc., can solve the problems of many control steps, complicated and complex preparation process of nickel oxide electrochromic film, and achieve good compactness and stability Good performance and good uniformity

Inactive Publication Date: 2004-09-15
HEFEI INST OF INTELLIGENT MACHINERY CHINESE ACAD OF SCI
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  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

However, the traditional formula for preparing nickel oxide sol is relatively complicated, which makes the preparation process of nickel oxide electrochromic thin film also very complicated, and the reaction needs to be controlled.

Method used

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  • Nickel oxide nano electrochromism film and preparing method thereof
  • Nickel oxide nano electrochromism film and preparing method thereof
  • Nickel oxide nano electrochromism film and preparing method thereof

Examples

Experimental program
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Embodiment Construction

[0027] (1), the preparation of nickel sol

[0028] 1. Mix 48ml of absolute ethanol and 12ml of butanol to obtain an organic solvent, and add 1.2g of NiCl under stirring 2 Reflux for half an hour when the temperature is raised to 76° C., add 1.2 g of distilled water, and continue to reflux for 1 hour to obtain nickel sol.

[0029] 2. Take 40ml absolute ethanol and 20ml amyl alcohol and mix to obtain an organic solvent, add 1.8g Ni(NO 3 ) 2 Reflux for half an hour when the temperature is raised to 80° C., add 0.36 g of citric acid and 1.8 g of distilled water, and continue to reflux for 1.5 hours to obtain nickel sol.

[0030] 3. Mix 35ml of absolute ethanol and 25ml of hexanol to obtain an organic solvent, add 2.4g of NiSO under stirring 4 Reflux for half an hour when the temperature is raised to 82°C, add 0.48g of glutaric acid and 2.4g of distilled water, and continue to reflux for 2 hours to obtain nickel sol.

[0031] (two), the preparation of nickel oxide thin film

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Abstract

The invention is nickel oxide nano electrochromism film and the manufacturing method, the method uses liquid-gelatum method to produce nickel colloidal sols, them the ITO glass piece is immersed into the liquid, and uses the film device to pull into film, the film can be get through drying, baking, quenching and cooling. The manufacturing method of colloidal sols uses inorganic nickel salt to dissolve in the compound organic solvent which uses waterless alcohol mainly, and they are back flowed every 78-82deg.C, then, adds in water and the organic acid to get the nickel colloidal sols. The invention is simple, the film is even, thick, the even particle radius is between 30-50mm, the light throughput varies in 7.9%-85%. The property of the product is stable.

Description

1. Technical field [0001] The invention relates to a color-changing thin film attached to a device and a preparation method thereof, in particular to a nickel oxide electrochromic thin film and a preparation method thereof. 2. Background technology [0002] There are many ways to prepare electrochromic thin films of nickel, including anodic oxidation, electrochemical deposition, electron beam evaporation, sputtering, high temperature direct oxidation and so on. However, these methods require large-scale equipment, the preparation process is complicated, and the film-forming area is limited by the equipment, so they are not suitable for large-scale preparation. [0003] At present, most of nickel oxide nano-electrochromic thin films are prepared by sol-gel method by hydrolysis of nickel alkoxide. However, the traditional formulations for preparing nickel oxide sol are relatively complicated, which makes the preparation process of nickel oxide electrochromic thin film also ve...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C09K11/00C09K11/60
Inventor 刘锦淮孟凡利王连超孙宇峰黄行九皮宗新
Owner HEFEI INST OF INTELLIGENT MACHINERY CHINESE ACAD OF SCI
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