Adsorption film material containing traditional Chinese medicine and preparation method thereof
A technology of membrane material and traditional Chinese medicine, applied in the field of health protection materials and its preparation, can solve the problems of virus insensitivity, limited antibacterial spectrum, high toxicity, etc., achieve strong killing of pathogenic microorganisms, good health protection performance, and good mechanical properties Effect
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Embodiment 1
[0013] 1. Preparation of adsorption film for active parts of traditional Chinese medicine compound
[0014] (1) Extract of active parts of traditional Chinese medicine compound
[0015] Chinese medicine prescription: Coptidis 50g, Forsythia 50g, Honeysuckle 50g, Scutellaria baicalensis 50g
[0016] 20g of the above-mentioned Chinese herbal medicines were respectively added with an appropriate amount of ethanol to soak for 3 days, percolated, repeated three times, filtered, and 20g of the extract concentrated from the percolated solution; the sample was mixed with silica gel, and the medium-pressure preparative chromatography was carried out, and the solvent was chloroform:petroleum (1-100% V / V) Gradient elution, the components were collected by an automatic component collector, 40-100% components were combined, and the solvent was recovered to obtain 8 g of active parts of the compound.
[0017] (2) The membrane material is polypropylene fiber membrane.
[0018] (3) Prepara...
Embodiment 2
[0027] 1. Preparation of adsorption film for active parts of traditional Chinese medicine compound
[0028] (1) Extract of active parts of traditional Chinese medicine compound
[0029] Chinese medicine prescription: Coptidis 50g, Forsythia 50g, Honeysuckle 50g, Scutellaria baicalensis 50g
[0030] 20g of the above-mentioned Chinese herbal medicines were respectively added with an appropriate amount of ethanol to soak for 3 days, percolated, repeated three times, filtered, and 20g of the extract concentrated from the percolated solution; the sample was mixed with silica gel, and the medium-pressure preparative chromatography was carried out, and the solvent was chloroform:petroleum (1-100% V / V) Gradient elution, the components were collected by an automatic component collector, 40-100% components were combined, and the solvent was recovered to obtain 8 g of active parts of the compound.
[0031] (2) The film material is polyvinyl alcohol fiber film.
[0032] (3) Preparation...
Embodiment 3
[0041] 1. Preparation of adsorption film for active parts of traditional Chinese medicine compound
[0042] (1) Extract of active parts of traditional Chinese medicine compound
[0043] Chinese medicine prescription: Coptidis 50g, Forsythia 50g, Honeysuckle 50g, Scutellaria baicalensis 50g
[0044] 20g of the above-mentioned Chinese herbal medicines were respectively added with an appropriate amount of ethanol to soak for 3 days, percolated, repeated three times, filtered, and 20g of the extract concentrated from the percolated solution; the sample was mixed with silica gel, and the medium-pressure preparative chromatography was carried out, and the solvent was chloroform:petroleum (1-100% V / V) Gradient elution, the components were collected by an automatic component collector, 40-100% components were combined, and the solvent was recovered to obtain 8 g of active parts of the compound.
[0045] (2) The membrane material is activated carbon fiber membrane.
[0046] (3) Prep...
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