Little interfered RNA preparation for internal preventing or curing respiratory system diseases and screening method thereof
A technology for respiratory diseases and screening methods, applied in the field of small interfering RNA preparations, can solve problems such as low cationic load
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Embodiment 1
[0069] Example 1: Preparation of cationic polymer / siRNA formulation. According to our research results at the cellular level, siRNA (see sequence listing) was synthesized by chemical methods (synthesis service provided by QIAGENE, Germany). Succinimide-based PEG3400 (PEG3400-N-hydroxy succinimide, purchased from Shearwater Polymers company) ( figure 2 ) was dissolved in 100mM HEPES (pH8) buffer solution, slowly added to PEI solution, kept stirring at room temperature for 5-9 hours, and the detected pH value was 9.5, left at room temperature for 4-6 days, freeze-dried the reaction product, and redissolved In 150mM NaCl (pH 7) solution prepared with 5mM HEPES, purified by gel column, dialyzed and ready for use. PEG-PEI and PEI were mixed at a ratio of 1:1 and dissolved in 5mM HEPES (pH8) buffer. The synthesized siRNA was also dissolved in 5mM HEPES (pH8) buffer. The two were mixed in a ratio of 2:1, and oscillated for 30 seconds.
Embodiment 2
[0070] Example 2: Preparation of cationic polypeptide / siRNA preparation.
[0071] Dissolve an appropriate amount of siRNA in RNase-free sterile water and mix gently. Due to the limited volume, a high concentration of siRNA can be used, generally 8-15 μg / μL for siRNA.
[0072] Take appropriate amount of siRNA and mix with cationic polypeptide (see sequence listing). SiRNA and cationic polypeptide were mixed at a ratio of 1:4-8, and incubated at room temperature for 30 minutes to form siRNA / cationic polypeptide complex. The prepared siRNA / cationic polypeptide complex can be used to introduce siRNA in vivo (including the respiratory system). This method is also applicable to in vivo introduction of DNA or DNA / siRNA complex.
Embodiment 3
[0073] Example 3: Preparation of nucleic acid protecting agent / siRNA preparation.
[0074] Dissolve an appropriate amount of siRNA (5-50 mg) in a solution of polyvinylpyrrolidine and glucose prepared by RNase-free sterile double-distilled water, and mix well at 4°C to make a complex of siRNA / nucleic acid protecting agent for use in Respiratory tract administration of siRNA.
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