Method for preparing Broussonetia papyrifera red pigment, and use thereof
A technology for constructing tree fruit and pigments, which is applied in the fields of food and beverages and medicine, and can solve the effects of liver function and transaminase index, the growth of sales is not as good, and the prevention, diagnosis, detection, protection, treatment and research of tree fruit pigments have not been found And other issues
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[0266] 2.1. Preparation of sarcocarp pigment Fresh and mature sarcocarp fruit was picked and identified by Professor Zheng Hanchen from the Pharmacy Teaching and Research Office of the Second Military Medical University. After drying, mash it into a pulp, add acetone to soak at room temperature, pour out the soaking liquid, add acetone again to soak until the pulp of mulberry fruit is colorless. The extracts are combined, filtered and distilled to recover acetone to obtain the fruit pigment product. Prepare 10% pigment aqueous solution with distilled water, and carry out TCL analysis. The developer is n-butanol: glacial acetic acid: water (4:1:5).
[0267] 2.2. Physicochemical properties of the fruit pigment
[0268] 2.2.1. Solubility The mulberry pigment is easily soluble in water, soluble in strong polar solvents such as methanol and acetic acid, and insoluble in weak polar organic solvents such as absolute ethanol, chloroform, benzene, and ether.
[0269] 2.2.2. Heat resi...
Embodiment 1
[0281] Embodiment 1, the preparation of fruit pigment powder injection
[0282] Take 38g of sarcocarp pigment, add 20g of methylcellulose, add 5000ml of water for injection, stir to dissolve; add water for injection to 10,000ml, add 3.0g of activated carbon for needles, stir for 30 minutes; decarbonize and filter; use 0.22μm Microporous membrane filtration; filling into sterile vials, 2ml per bottle, half-stoppered; freeze-dried, then cork and cover.
Embodiment 2
[0283] Embodiment 2, the preparation of fruit pigment powder injection
[0284] (1) Prescription
[0285] Marigold Pigment for Injection 38g
[0286] Mannitol 40g
[0287] Add water for injection to 10000ml
[0288] A total of 5000 bottles were made
[0289] (2) Preparation process
[0290] According to the above prescription, take the prescribed amount of fruit pigment, add it to an appropriate amount of water for injection, stir to dissolve it; add the prescribed amount of mannitol, stir it to dissolve completely, add water for injection to the full amount; add 0.1% liquid amount of activated carbon for injection , fully stirred for 30 minutes; decarbonized and filtered; filtered with a 0.22 μm microporous membrane; filled, half-plugged; freeze-dried, plugged and capped. A total of 4867 bottles were produced, with a yield of 97.35%.
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