Composition for forming underlying film containing dextrin ester compound
A compound, dextrin ester technology, which is applied in the photoengraving process of the pattern surface, the photosensitive material for opto-mechanical equipment, optics, etc., can solve the problem that the anti-reflection film material is difficult to apply to the substrate, etc., and achieve high filling. , the effect of good precision
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Embodiment
[0090] Dextrin ester compound AC-3 (the terminal group ratio of dextrin: 24% of hydroxyl group, 76% of acetoxy group, weight average molecular weight of 8100, produced by Qunyei Chemical Industry Co., Ltd. ), add 9.23g of tetramethoxymethyl glycoluril, 0.01g of pyridinium p-toluenesulfonate, 0.129g of surfactant R-30 (manufactured by Dainippon Inki Chemical Co., Ltd.), 14.79g g of propylene glycol monomethyl ether, and 73.91 g of ethyl lactate to form an 18.0% by mass solution. Then, it was filtered using a polyethylene microfilter with a pore size of 0.05 μm to prepare a solution of a composition for forming a lower layer membrane.
[0091] In addition, the terminal group ratio of dextrin: 24% of hydroxyl groups and 76% of acetoxy groups means that 76% of the total number of hydroxyl groups contained in dextrin are acetoxy groups and the remaining 24% are hydroxyl groups.
[0092] In addition, the weight average molecular weight of a dextrin ester compound is measured by the...
Embodiment 2
[0095] Dextrin ester compound AC-4 (the terminal group ratio of dextrin: hydroxyl 32%, acetoxy 68%, weight average molecular weight 8900, manufactured by Qunyei Chemical Industry Co., Ltd.) with a concentration of 30% by mass was dissolved in 85.0 g ), add 9.23g of tetramethoxymethyl glycoluril, 0.01g of pyridinium p-toluenesulfonate, 0.129g of surfactant R-30 (manufactured by Dainippon Inki Chemical Co., Ltd.), 14.79g g of propylene glycol monomethyl ether, and 73.91 g of ethyl lactate to form an 18.0% by mass solution. Then, it was filtered using a polyethylene microfilter with a pore size of 0.05 μm to prepare a solution of a composition for forming a lower layer membrane.
Embodiment 3
[0097] Dextrin ester compound AC-3 (the terminal group ratio of dextrin: 24% of hydroxyl group, 76% of acetoxy group, weight average molecular weight of 8100, produced by Qunyei Chemical Industry Co., Ltd. ) in ethyl lactate solution, add 9.23g tetramethoxymethyl glycoluril, 0.0271g ammonium dodecylbenzenesulfonate, 0.129g surfactant R-30 (manufactured by Dainippon Inki Chemical Co., Ltd.) , 14.79 g of propylene glycol monomethyl ether, and 73.91 g of ethyl lactate to form a solution of 18.0% by mass. Then, it was filtered using a polyethylene microfilter with a pore size of 0.05 μm to prepare a solution of a composition for forming a lower layer membrane.
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