Aqueous dispersoid for chemical machinery grinding and grinding method and concocting reagent kit
A chemical-mechanical and dispersion technology, applied in chemical instruments and methods, polishing compositions containing abrasives, grinding devices, etc., can solve problems such as scratches or peeling of semiconductor substrates, low mechanical strength, and product yield problems, To achieve the effect of reducing scratches or peeling
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Embodiment 1
[0232] 3.2.1. Preparation of the second grinding water-based dispersion (the chemical mechanical polishing water-based dispersion of the first form of the present invention)
[0233]Water containing colloidal silica particles C1 prepared in the above "3.1.2-1. Preparation of aqueous dispersion containing colloidal silica particles C1" in an amount equivalent to 1% by mass in terms of silica Dispersion, and the aqueous dispersion containing organic-inorganic composite particles prepared in the above "3.1.3. Preparation of aqueous dispersion containing organic-inorganic composite particles" in an amount corresponding to 0.1% by mass in terms of organic-inorganic composite particles Put into a bottle made of polyethylene, add 0.2% by mass of benzotriazole, 0.1% by mass of maleic acid, and 35% by mass of hydrogen peroxide water in an amount equivalent to 0.3% by mass in terms of hydrogen peroxide in this order, and stir for 15 minutes. Next, ion-exchanged water was added until th...
Embodiment 2~5
[0292] 3.3. Examples 2-5, Comparative Examples 1-2
[0293] Except that the kind and the addition amount of each component of the second grinding water-based dispersion in Example 1 and the pH of the water-based dispersion are set as in Table 2, other experiments were carried out in the same manner as in Example 1, and the No. 2. Grinding water-based dispersions S2-S5 and R1-R2. In addition, in Table 2, "-" means that the component corresponding to the corresponding column was not added. In addition, Example 4 used two types of particles as (B) component, and Example 5 used two types of particles as (A) component.
[0294] As the second polishing water-based dispersion, evaluation was performed in the same manner as in Example 1, except that each of the above-synthesized water-based dispersions was used instead of S1. The results are shown in Table 3.
[0295] Water system
[0296] Example 1
[0297] According to Table 2 and Table 3, it can be seen t...
Embodiment 6
[0299] 3.4.1. Preparation of the second grinding water-based dispersion (a kit for preparing the chemical mechanical grinding water-based dispersion of the first form of the present invention)
[0300] 3.4.1-1. Preparation of liquid (I)
[0301] Water containing colloidal silica particles C1 prepared in the above "3.1.2-1. Preparation of aqueous dispersion containing colloidal silica particles C1" in an amount equivalent to 1.06% by mass in terms of silica Dispersion, and the aqueous dispersion containing organic-inorganic composite particles prepared in the above "3.1.3. Preparation of aqueous dispersion containing organic-inorganic composite particles" in an amount corresponding to 0.11% by mass in terms of organic-inorganic composite particles It was put into a polyethylene bottle, 0.21% by mass of benzotriazole and maleic acid in an amount corresponding to 0.11% by mass were sequentially added thereto, and stirred for 15 minutes. Next, ion-exchanged water was added until ...
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