Method for producing antibacterial polylactic acid fiber
A technology of polylactic acid fiber and production method, applied in the direction of fiber chemical characteristics, single-component polyester rayon, textiles and papermaking, etc., can solve the problems that have not yet been developed and produced antibacterial polylactic acid fiber, etc., and achieve high fiber quality , Good effect of spinning and forming
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Embodiment 1
[0013] Embodiment one: the treatment of antibacterial powder
[0014] Get 2Kg mean particle diameter and be the silver-containing inorganic antibacterial superfine powder (HN-300 of 0.25 micron; Jiangsu Hehai Nano Material Co., Ltd. production), put into vacuum drying oven, dry 4 hours under 130 ℃, the above-mentioned Put the powder into a 20-liter high-speed kneader, add 80 g of 25% ethanol solution of sodium petroleum sulfonate, and knead it for 100 minutes at 300 rpm, then put it into a vacuum drying oven and dry it at 100°C for 10 hours. The surface-treated functional antibacterial powder is obtained.
[0015] or--
[0016] Get 2Kg of silver-containing inorganic antibacterial superfine powders (HN-300; produced by Jiangsu Hehai Nano Materials Co., Ltd.) with an average particle size of 0.5 microns, put them in a vacuum drying oven, and dry them at 110°C for 6 hours. Put the powder into a 20-liter high-speed kneader, add 70g of 35% ethanol solution of potassium dodecyl ph...
Embodiment 2
[0017] Embodiment 2: Preparation of antibacterial polylactic acid masterbatch
[0018] Dry the pulverized 8Kg polylactic acid slices at 110°C for 20 hours, mix them with the 2Kg antibacterial powder after the above treatment, and add 100 grams of 60# paraffin as a lubricant. Extrude and granulate to obtain polylactic acid masterbatch with antibacterial function.
Embodiment 3
[0019] Embodiment 3: Production and manufacture of antibacterial polylactic acid fiber
[0020] Drying of slices: First, accurately measure polylactic acid slices and antibacterial masterbatches, add them to the vacuum drying equipment at a ratio of 50:1, dry them in vacuum at 95°C for 10 hours, then heat them up to 110°C and dry them in vacuum for 4 hours, then cool them down to 90°C in vacuum Dry for 2 hours.
[0021] Spinning: on the composite spinning machine (manufactured by Japan ABE Company), spinning is carried out with 240 ℃ of spinning temperatures, 1200M / min of winding speed, then on the Barmag3013 drafting machine, carry out drafting post-processing, draft ratio 3.5, The temperature of the hot plate is 80°C, and the temperature of the hot plate is 130°C to prepare antibacterial polylactic acid fibers.
[0022] The antibacterial test of the antibacterial polylactic acid fiber prepared by spinning shows that the antibacterial rate of the antibacterial polylactic aci...
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