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Process for extracting total saponin from papermulberry fruit

A technology for extracting saponins from the fruit of the fruit and total saponins, which is applied in the field of extracting saponins, and can solve the problems of failure to extract the saponins from the fruit of the fruit, low saponin content, and low purity of saponins

Inactive Publication Date: 2007-07-04
贵州三农楮桃产业开发有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Due to the low content of saponins in the fruit, the extraction rate of active ingredients by traditional methods is low, and the purity of saponins obtained is not high
Therefore, people have not been able to extract mulberry saponins for health care and medical treatment

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment Construction

[0012] Embodiments of the invention. The method for extracting saponins is prepared by the following steps.

[0013] a. After dried and pulverized, the mulberry seed is passed through a 50-mesh sieve to obtain the mulberry seed powder, which is product A.

[0014] b. Separating the mulberry seed powder through mechanical pressing to separate the mulberry peach oil; or putting the mulberry seed powder into CO 2 In the supercritical extraction device, control the pressure at 10mpa-20mpa and extract at a temperature of 40-50°C. Extract and separate the mulberry oil; the remaining mixture is product B.

[0015] c. Refining and extracting product B with 95% edible alcohol through a Soxhlet extractor to obtain product C.

[0016] The content of saponins extracted by the method of the present invention is high, and the content of total saponins in the fruit of C. product is 51.8% after testing.

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PUM

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Abstract

The invention discloses a method which extracts total soap glucoside from papermulberry fruit. It follows below steps to preparing: drying and disintegrating the papermulberry fruit and getting the papermulberry fruit powder as A material; extracting A material through mechanical squeeze or carbon dioxide supercritical extraction device, separating the papermulberry fruit peach oil and the resulting mixture is B material; extracting and refinishing B material with organic solvent and getting papermulberry fruit total soap glucoside. The invention uses mechanical squeeze or carbon dioxide supercritical extraction device to removing papermulberry fruit peach oil, then refines and extracts the material using flavouring alcohol, the got total soap glucoside extraction rate >=1.84% which is higher then other methods extraction rate(0.51%) in prior technology 3.5 times. At the same time it solves the question of effective ingredients easily lost better, raises the rate of extraction but also solves the problems of removing impurities, improving purity and decreasing cost while increasing the rate of extraction, so achieves the purpose of the invention. The extracted papermulberry fruit total soap glucoside has many effects and can be used as processing raw materials of medicines and health products.

Description

technical field [0001] The invention relates to a method for extracting saponins from plant seeds, in particular to a method for extracting total saponins from mulberry seeds. Background technique [0002] Sulmus mulberry, also known as mulberry tree, lemon wood, deciduous tree (Broussonetia papyrifera (L.) vent) of Moraceae plants, dioecious, distributed in most parts of the country, growing on hillsides, ravines, mostly wild, with a small amount cultivation. "Compendium of Materia Medica" claims that its fruit (Chushi) has the functions of "nourishing yin and tonifying kidney, clearing liver and improving eyesight, long-term use without muscle aging, light body and strong bones, boosting yang energy, tonifying deficiency and tuberculosis, strengthening waist and knees, and benefiting color" and other functions effect. According to the research of modern technology, the fruit of the mulberry tree (the seed of the mulberry tree) contains saponin and the fruit of the saponi...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): A61K36/60C07G3/00
CPCY02P20/54
Inventor 黄大建谢筠郁李海滨莫彬彬
Owner 贵州三农楮桃产业开发有限公司
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