Negative-electrode active material for nonaqueous-electrolyte secondary battery production process for the same, negative electrode for nonaqueous-electrolyte secondary battery, and nonaqueous-electrolyte secondary battery
a nonaqueouselectrolyte and active material technology, applied in the direction of carbon-silicon compound conductors, non-conductive materials with dispersed conductive materials, cell components, etc., can solve the problems of reducing the electrical resistance of negative electrodes. , to achieve the effect of reducing the electric resistance, enhancing the conductivity of lithium ion, and lowering the electric resistance resistan
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[0092]The present invention is hereinafter described concretely, while giving an embodiment thereof.
Manufacture of Coin-Type Lithium-Ion Secondary Battery
[0093]Nanometer-size Si particles (produced by HAMAMATSU NANOTECHNOLOGY Co., Ltd.) with 50-nm average particle diameter was readied as nanometer-size Si particles. Polyamide-imide resin produced by SIGMA-ALDRICH JAPAN Limited Liability Company was readied. Copper phthalocyanine produced by SIGMA-ALDRICH JAPAN Limited Liability Company was readied.
first embodiment
[0094]50-part-by-mass nanometer-size Si particles, 10-part-by-mass polyamide-imide resin, and 10-part-by-mass copper phthalocyanine were weighed out. The nanometer-size Si particles, polyamide-imide resin, and copper phthalocyanine were added to 30-part-by-mass N-methyl-2-pyrrolidone (or NMP produced by SIGMA-ALDRICH JAPAN Limited Liability Company). The resulting mixture was put in an agate mortar, and was then kneaded. The resultant kneaded substance was dried at 100° C. for 1 hour, thereby removing the NMP from the kneaded substance.
[0095]The kneaded substance from which the NMP had been excluded was heated at 800° C. for 1 hour under an argon atmosphere, thereby obtaining an Si—Cu-carbon composite according to First Embodiment. When the Si—Cu-carbon composite according to First Embodiment was taken as 100% by mass, a content rate of the nanometer-size Si particles was about 60% by mass. The content rate of the nanometer-size Si particles was computed by actually measuring the va...
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